dimethyl [(1R)-1-{[(R)-(tert-butyl)sulfinyl]amino}-3-phenylpropyl]propanedioate

Base Information

Chemical Name:dimethyl [(1R)-1-{[(R)-(tert-butyl)sulfinyl]amino}-3-phenylpropyl]propanedioate
CAS No.:1412429-46-9
Molecular Formula:C₁₈H₂₇NO₅S
Molecular Weight:369.482
Hs Code.:

Synonyms:dimethyl [(1R)-1-{[(R)-(tert-butyl)sulfinyl]amino}-3-phenylpropyl]propanedioate

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Chemical Property of dimethyl [(1R)-1-{[(R)-(tert-butyl)sulfinyl]amino}-3-phenylpropyl]propanedioate

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Technology Process of dimethyl [(1R)-1-{[(R)-(tert-butyl)sulfinyl]amino}-3-phenylpropyl]propanedioate

There total 2 articles about dimethyl [(1R)-1-{[(R)-(tert-butyl)sulfinyl]amino}-3-phenylpropyl]propanedioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 508225-73-8
(R)-N-(tert-butanesulfinyl)-N-(3-phenylpropyliden)amine

: 108-59-8
malonic acid dimethyl ester

: 1412429-46-9
dimethyl [(1R)-1-{[(R)-(tert-butyl)sulfinyl]amino}-3-phenylpropyl]propanedioate

Guidance literature:: With sodium iodide; at 23 ℃; for 72h; diastereoselective reaction;
DOI:10.1002/hlca.201200303 DOI:10.1002/hlca.201200303

Reference yield:

: 508225-73-8
(R)-N-(tert-butanesulfinyl)-N-(3-phenylpropyliden)amine

: 108-59-8
malonic acid dimethyl ester

: 1412429-46-9
dimethyl [(1R)-1-{[(R)-(tert-butyl)sulfinyl]amino}-3-phenylpropyl]propanedioate

: 1412429-47-0
dimethyl [(1S)-1-{[(R)-(tert-butyl)sulfinyl]amino}-3-phenylpropyl]propanedioate

Guidance literature:: With potassium tert-butylate; In tetrahydrofuran; at 23 ℃; for 72h;
DOI:10.1002/hlca.201200303 DOI:10.1002/hlca.201200303

Reference yield: 82.0%

: 1412429-46-9
dimethyl [(1R)-1-{[(R)-(tert-butyl)sulfinyl]amino}-3-phenylpropyl]propanedioate

: 103123-47-3
methyl (3R)-3-amino-5-phenylpentanoate

Guidance literature:: With hydrogenchloride; In methanol; water; at 20 - 100 ℃; for 37.5h;
DOI:10.1002/hlca.201200303 DOI:10.1002/hlca.201200303