benzyl 2-N-acetyl-3,6-di-O-benzyl-2-deoxy-5-O-methyl-α-D-mannofuranoside

Base Information

Chemical Name:benzyl 2-N-acetyl-3,6-di-O-benzyl-2-deoxy-5-O-methyl-α-D-mannofuranoside
CAS No.:119870-40-5
Molecular Formula:C₃₀H₃₅NO₆
Molecular Weight:505.611
Hs Code.:

Synonyms:benzyl 2-N-acetyl-3,6-di-O-benzyl-2-deoxy-5-O-methyl-α-D-mannofuranoside

Suppliers and Price of benzyl 2-N-acetyl-3,6-di-O-benzyl-2-deoxy-5-O-methyl-α-D-mannofuranoside

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of benzyl 2-N-acetyl-3,6-di-O-benzyl-2-deoxy-5-O-methyl-α-D-mannofuranoside

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of benzyl 2-N-acetyl-3,6-di-O-benzyl-2-deoxy-5-O-methyl-α-D-mannofuranoside

There total 10 articles about benzyl 2-N-acetyl-3,6-di-O-benzyl-2-deoxy-5-O-methyl-α-D-mannofuranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 119870-63-2
benzyl 2-azido-3,6-di-O-benzyl-2-deoxy-5-O-methyl-α-D-mannofuranoside

: 507-09-5
tiolacetic acid

: 119870-40-5
benzyl 2-N-acetyl-3,6-di-O-benzyl-2-deoxy-5-O-methyl-α-D-mannofuranoside

Guidance literature:: With pyridine; at 0 - 20 ℃;
DOI:10.1016/j.bmcl.2011.04.083

Reference yield:

: 1332835-21-8
benzyl 3-O-benzyl-5,6-carbonate-α-D-glucofuranoside

: 119870-40-5
benzyl 2-N-acetyl-3,6-di-O-benzyl-2-deoxy-5-O-methyl-α-D-mannofuranoside

Guidance literature:: Multi-step reaction with 6 steps

1.1: pyridine / dichloromethane / 0.5 h / -30 °C

2.1: sodium azide / N,N-dimethyl-formamide / 0 - 20 °C

3.1: sodium methylate / methanol / 20 °C

4.1: di(n-butyl)tin oxide / toluene / 2 h / Reflux

4.2: 24 h / Inert atmosphere; Reflux

5.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.33 h

5.2: 20 °C

6.1: pyridine / 0 - 20 °C

With pyridine; sodium azide; sodium methylate; sodium hydride; di(n-butyl)tin oxide; In methanol; dichloromethane; N,N-dimethyl-formamide; toluene; mineral oil;
DOI:10.1016/j.bmcl.2011.04.083

Reference yield:

: 1332835-23-0
benzyl 2-azido-3,6-di-O-benzyl-2-deoxy-α-D-mannofuranoside

: 119870-40-5
benzyl 2-N-acetyl-3,6-di-O-benzyl-2-deoxy-5-O-methyl-α-D-mannofuranoside

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.33 h

1.2: 20 °C

2.1: pyridine / 0 - 20 °C

With pyridine; sodium hydride; In N,N-dimethyl-formamide; mineral oil;
DOI:10.1016/j.bmcl.2011.04.083