(S)-N-(4-(1-acetyl-5-(4-methoxyphenyl)-4,5-dihydro-1H-pyrazol-3-yl)phenyl)-4-fluorobenzenesulfonamide

Base Information

Chemical Name:(S)-N-(4-(1-acetyl-5-(4-methoxyphenyl)-4,5-dihydro-1H-pyrazol-3-yl)phenyl)-4-fluorobenzenesulfonamide
CAS No.:1415031-29-6
Molecular Formula:C₂₄H₂₂FN₃O₄S
Molecular Weight:467.521
Hs Code.:

Synonyms:(S)-N-(4-(1-acetyl-5-(4-methoxyphenyl)-4,5-dihydro-1H-pyrazol-3-yl)phenyl)-4-fluorobenzenesulfonamide

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Chemical Property of (S)-N-(4-(1-acetyl-5-(4-methoxyphenyl)-4,5-dihydro-1H-pyrazol-3-yl)phenyl)-4-fluorobenzenesulfonamide

Chemical Property:

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Technology Process of (S)-N-(4-(1-acetyl-5-(4-methoxyphenyl)-4,5-dihydro-1H-pyrazol-3-yl)phenyl)-4-fluorobenzenesulfonamide

There total 7 articles about (S)-N-(4-(1-acetyl-5-(4-methoxyphenyl)-4,5-dihydro-1H-pyrazol-3-yl)phenyl)-4-fluorobenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1415031-27-4
N-(4-(1-acetyl-5-(4-methoxyphenyl)-4,5-dihydro-1H-pyrazol-3-yl)phenyl)-4-fluorobenzenesulfonamide

: 1415031-28-5
(R)-N-(4-(1-acetyl-5-(4-methoxyphenyl)-4,5-dihydro-1H-pyrazol-3-yl)phenyl)-4-fluorobenzenesulfonamide

: 1415031-29-6
(S)-N-(4-(1-acetyl-5-(4-methoxyphenyl)-4,5-dihydro-1H-pyrazol-3-yl)phenyl)-4-fluorobenzenesulfonamide

Guidance literature:: With CHIRALPAK AD-H 4.6*250 mm 5 um (Daicel); In methanol; carbon dioxide; at 40 ℃; under 112511 Torr; Product distribution / selectivity; Resolution of racemate; Supercritical fluid chromatography;

Reference yield:

: 99-92-3
p-aminobenzophenone

: 1415031-28-5
(R)-N-(4-(1-acetyl-5-(4-methoxyphenyl)-4,5-dihydro-1H-pyrazol-3-yl)phenyl)-4-fluorobenzenesulfonamide

: 1415031-29-6
(S)-N-(4-(1-acetyl-5-(4-methoxyphenyl)-4,5-dihydro-1H-pyrazol-3-yl)phenyl)-4-fluorobenzenesulfonamide

Guidance literature:: Multi-step reaction with 6 steps

1: pyridine / 20 °C

2: sulfuric acid / methanol / Reflux

3: hydrazine; pyridine / ethanol / 3 h / Reflux

4: pyridine / 2 h / 20 °C

5: ammonium hydroxide / ethanol / 2 h / 20 °C

6: CHIRALPAK AD-H 4.6*250 mm 5 um (Daicel) / carbon dioxide; methanol / 40 °C / 112511 Torr / Resolution of racemate; Supercritical fluid chromatography

With pyridine; ammonium hydroxide; hydrazine; sulfuric acid; In methanol; ethanol; carbon dioxide;

Reference yield:

: 349-88-2
4-Fluorobenzenesulfonyl chloride

: 1415031-28-5
(R)-N-(4-(1-acetyl-5-(4-methoxyphenyl)-4,5-dihydro-1H-pyrazol-3-yl)phenyl)-4-fluorobenzenesulfonamide

: 1415031-29-6
(S)-N-(4-(1-acetyl-5-(4-methoxyphenyl)-4,5-dihydro-1H-pyrazol-3-yl)phenyl)-4-fluorobenzenesulfonamide

Guidance literature:: Multi-step reaction with 6 steps

1: pyridine / 20 °C

2: sulfuric acid / methanol / Reflux

3: hydrazine; pyridine / ethanol / 3 h / Reflux

4: pyridine / 2 h / 20 °C

5: ammonium hydroxide / ethanol / 2 h / 20 °C

6: CHIRALPAK AD-H 4.6*250 mm 5 um (Daicel) / carbon dioxide; methanol / 40 °C / 112511 Torr / Resolution of racemate; Supercritical fluid chromatography

With pyridine; ammonium hydroxide; hydrazine; sulfuric acid; In methanol; ethanol; carbon dioxide;