Technology Process of ethyl 3-cyano-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzoate
There total 4 articles about ethyl 3-cyano-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzoate which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2; potassium acetate;
In
dimethyl sulfoxide;
at 80 ℃;
for 4h;
Schlenk technique;
Inert atmosphere;
DOI:10.1021/acs.jmedchem.6b00829
- Guidance literature:
-
Multi-step reaction with 3 steps
1: sulfuric acid / 5 h / 90 °C
2: tetrakis(triphenylphosphine) palladium(0) / N,N-dimethyl-formamide / 1 h / 80 °C / Inert atmosphere
3: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2; potassium acetate / dimethyl sulfoxide / 4 h / 80 °C / Schlenk technique; Inert atmosphere
With
tetrakis(triphenylphosphine) palladium(0); dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2; sulfuric acid; potassium acetate;
In
dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1021/acs.jmedchem.6b00829