2-<(2S,4S)-3-Benzoyl-2-(tert-butyl)-1-methyl-5-oxoimidazolidin-4-yl>essigsaeure

Base Information

Chemical Name:2-<(2S,4S)-3-Benzoyl-2-(tert-butyl)-1-methyl-5-oxoimidazolidin-4-yl>essigsaeure
CAS No.:103825-46-3
Molecular Formula:C₁₇H₂₂N₂O₄
Molecular Weight:318.373
Hs Code.:

Synonyms:2-<(2S,4S)-3-Benzoyl-2-(tert-butyl)-1-methyl-5-oxoimidazolidin-4-yl>essigsaeure

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Chemical Property of 2-<(2S,4S)-3-Benzoyl-2-(tert-butyl)-1-methyl-5-oxoimidazolidin-4-yl>essigsaeure

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Technology Process of 2-<(2S,4S)-3-Benzoyl-2-(tert-butyl)-1-methyl-5-oxoimidazolidin-4-yl>essigsaeure

There total 4 articles about 2-<(2S,4S)-3-Benzoyl-2-(tert-butyl)-1-methyl-5-oxoimidazolidin-4-yl>essigsaeure which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.4%

: 103825-42-9
2-<(2S,4S)-3-Benzoyl-2-(tert-butyl)-1-methyl-5-oxoimidazolidin-4-yl>essigsaeure-methylester

: 103825-46-3
2-<(2S,4S)-3-Benzoyl-2-(tert-butyl)-1-methyl-5-oxoimidazolidin-4-yl>essigsaeure

Guidance literature:: With potassium hydroxide; In methanol; water; 1.) 0 deg C, 15 min; 2.) room temperature, 10 h;
DOI:10.1002/hlca.19850680603

Reference yield:

: 98-88-4
benzoyl chloride

: 103825-46-3
2-<(2S,4S)-3-Benzoyl-2-(tert-butyl)-1-methyl-5-oxoimidazolidin-4-yl>essigsaeure

Guidance literature:: Multi-step reaction with 2 steps

1: 31.7 percent / Et₃N / CH₂Cl₂ / 1.) 0 deg C 45 min; 2.) room temperature 12 h

2: 99.4 percent / KOH / methanol; H₂O / 1.) 0 deg C, 15 min; 2.) room temperature, 10 h

With potassium hydroxide; triethylamine; In methanol; dichloromethane; water;
DOI:10.1002/hlca.19850680603

Reference yield:

: 630-19-3
pivalaldehyde

: 103825-46-3
2-<(2S,4S)-3-Benzoyl-2-(tert-butyl)-1-methyl-5-oxoimidazolidin-4-yl>essigsaeure

Guidance literature:: Multi-step reaction with 3 steps

2: 31.7 percent / Et₃N / CH₂Cl₂ / 1.) 0 deg C 45 min; 2.) room temperature 12 h

3: 99.4 percent / KOH / methanol; H₂O / 1.) 0 deg C, 15 min; 2.) room temperature, 10 h

With potassium hydroxide; triethylamine; In methanol; dichloromethane; water;
DOI:10.1002/hlca.19850680603