trans-(meso-tetra-p-tolylporphyrinato)Ti(THF)2

Base Information

Chemical Name:trans-(meso-tetra-p-tolylporphyrinato)Ti(THF)2
CAS No.:199998-28-2
Molecular Formula:C₅₆H₅₂N₄O₂Ti
Molecular Weight:860.934
Hs Code.:

Synonyms:trans-(meso-tetra-p-tolylporphyrinato)Ti(THF)2

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Chemical Property of trans-(meso-tetra-p-tolylporphyrinato)Ti(THF)2

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Technology Process of trans-(meso-tetra-p-tolylporphyrinato)Ti(THF)2

There total 3 articles about trans-(meso-tetra-p-tolylporphyrinato)Ti(THF)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.3%

: 109-99-9,24979-97-3,77392-70-2
tetrahydrofuran

: 129679-90-9
(meso-tetra-p-tolylporphyrinato)titanium(III) chloride

: 199998-28-2
trans-(meso-tetra-p-tolylporphyrinato)Ti(THF)2

Guidance literature:: With CH₂CHCH₂MgCl; In tetrahydrofuran; toluene; byproducts: allyl radical dimer, MgCl2; absence of air and moisture; dropwise addn. of Grignard reagent (in THF)to Ti-complex (in PhMe) with stirring, standing for 18 h; solvent removal (reduced pressure), extn. into PhMe, filtration (Celite), solvent removal (reduced pressure), trituration with hexanes, solvent removal; can be crystallized (diffusion of hexanes into PhMe soln.); elem. anal.;