10-Undecenyl 2,3,4,6-tetra-O-benzyl-β-D-glucopyranoside

Base Information

Chemical Name:10-Undecenyl 2,3,4,6-tetra-O-benzyl-β-D-glucopyranoside
CAS No.:160062-76-0
Molecular Formula:C₄₅H₅₆O₆
Molecular Weight:692.936
Hs Code.:

Synonyms:10-Undecenyl 2,3,4,6-tetra-O-benzyl-β-D-glucopyranoside

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Chemical Property of 10-Undecenyl 2,3,4,6-tetra-O-benzyl-β-D-glucopyranoside

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Technology Process of 10-Undecenyl 2,3,4,6-tetra-O-benzyl-β-D-glucopyranoside

There total 4 articles about 10-Undecenyl 2,3,4,6-tetra-O-benzyl-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 100-39-0
benzyl bromide

: 134078-53-8
1-O-(undec-10-enyl) β-D-glucopyranoside

: 160062-76-0
10-Undecenyl 2,3,4,6-tetra-O-benzyl-β-D-glucopyranoside

Guidance literature:: With sodium hydride;
DOI:10.1080/07328309608005433

Reference yield:

: 572-09-8,3068-32-4,4026-32-8,6919-96-6,13242-53-0,14227-54-4,14795-18-7,19186-59-5,19285-38-2,21698-13-5,29907-26-4,53369-42-9,60619-58-1,61303-35-3,67337-79-5,69127-37-3,70749-15-4,72002-90-5,75247-30-2,75880-74-9,78418-57-2,102339-89-9,102339-90-2,103530-40-1,114028-03-4,114718-45-5,138514-70-2,138514-71-3
2,3,4,6-tetra-O-acetyl-D-glucopyranosyl bromide

: 160062-76-0
10-Undecenyl 2,3,4,6-tetra-O-benzyl-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 67 percent / AgOTf, molecular sieves / CH₂Cl₂ / Ambient temperature

2: 95 percent / K₂CO₃, MeOH / 4 h / Ambient temperature

3: 63 percent / NaH

With methanol; molecular sieve; silver trifluoromethanesulfonate; sodium hydride; potassium carbonate; In dichloromethane;
DOI:10.1080/07328309608005433

Reference yield:

: 112-43-6
10-Undecen-1-ol

: 160062-76-0
10-Undecenyl 2,3,4,6-tetra-O-benzyl-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 67 percent / AgOTf, molecular sieves / CH₂Cl₂ / Ambient temperature

2: 95 percent / K₂CO₃, MeOH / 4 h / Ambient temperature

3: 63 percent / NaH

With methanol; molecular sieve; silver trifluoromethanesulfonate; sodium hydride; potassium carbonate; In dichloromethane;
DOI:10.1080/07328309608005433