1,2,3,4-tetrahydro-1,4-methanonaphthalene-1,2-endo,3-endo-tricarboxylic acid N-phenyl-2,3-dicarboximide

Base Information

Chemical Name:1,2,3,4-tetrahydro-1,4-methanonaphthalene-1,2-endo,3-endo-tricarboxylic acid N-phenyl-2,3-dicarboximide
CAS No.:74143-72-9
Molecular Formula:C₂₀H₁₅NO₄
Molecular Weight:333.343
Hs Code.:

Synonyms:1,2,3,4-tetrahydro-1,4-methanonaphthalene-1,2-endo,3-endo-tricarboxylic acid N-phenyl-2,3-dicarboximide

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Chemical Property of 1,2,3,4-tetrahydro-1,4-methanonaphthalene-1,2-endo,3-endo-tricarboxylic acid N-phenyl-2,3-dicarboximide

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Technology Process of 1,2,3,4-tetrahydro-1,4-methanonaphthalene-1,2-endo,3-endo-tricarboxylic acid N-phenyl-2,3-dicarboximide

There total 2 articles about 1,2,3,4-tetrahydro-1,4-methanonaphthalene-1,2-endo,3-endo-tricarboxylic acid N-phenyl-2,3-dicarboximide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

: 941-69-5
N-phenyl-maleimide

: 14209-41-7
3H-indene-1-carboxylic acid

: 74143-72-9
1,2,3,4-tetrahydro-1,4-methanonaphthalene-1,2-endo,3-endo-tricarboxylic acid N-phenyl-2,3-dicarboximide

Guidance literature:: In xylene; for 9h; Heating;
DOI:10.1021/jo01305a017

Reference yield:

: 95-13-6
1-indene

: 74143-72-9
1,2,3,4-tetrahydro-1,4-methanonaphthalene-1,2-endo,3-endo-tricarboxylic acid N-phenyl-2,3-dicarboximide

Guidance literature:: Multi-step reaction with 2 steps

1: 1) 1-butyllithium / 1) hexane, diethyl ether, reflux, 1 h, 2) -78 deg C to room temperature

2: 46 percent / xylene / 9 h / Heating

With n-butyllithium; In xylene;
DOI:10.1021/jo01305a017