diethyl 5-[3-(benzyloxy)propyl]nonanedioate

Base Information

Chemical Name:diethyl 5-[3-(benzyloxy)propyl]nonanedioate
CAS No.:1187663-05-3
Molecular Formula:C₂₃H₃₆O₅
Molecular Weight:392.536
Hs Code.:

Synonyms:diethyl 5-[3-(benzyloxy)propyl]nonanedioate

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Chemical Property of diethyl 5-[3-(benzyloxy)propyl]nonanedioate

Chemical Property:

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Technology Process of diethyl 5-[3-(benzyloxy)propyl]nonanedioate

There total 6 articles about diethyl 5-[3-(benzyloxy)propyl]nonanedioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4541-14-4
4-benzyloxy-butan-1-ol

: 1187663-05-3
diethyl 5-[3-(benzyloxy)propyl]nonanedioate

Guidance literature:: Multi-step reaction with 6 steps

1.1: Jones reagent / acetone

2.1: sulfuric acid / 12 h / Reflux

3.1: iodine; magnesium / diethyl ether / 2 h / Inert atmosphere; Reflux

3.2: 5 h / Inert atmosphere; Reflux

4.1: ammonium cerium (IV) nitrate / water; acetonitrile / 6 h / Cooling with ice

5.1: Jones reagent / acetone

6.1: sulfuric acid / 12 h / Reflux

6.2: 6 h / 20 °C / 760.05 Torr

With Jones reagent; ammonium cerium (IV) nitrate; sulfuric acid; iodine; magnesium; In diethyl ether; water; acetone; acetonitrile; 1.1: Jones oxidation / 5.1: Jones oxidation;
DOI:10.1002/asia.201100480

Reference yield:

: 64-17-5
ethanol

: C₁₉H₂₈O₆

: 1187663-05-3
diethyl 5-[3-(benzyloxy)propyl]nonanedioate

Guidance literature:: ethanol; C₁₉H₂₈O₆; With sulfuric acid; for 12h; Reflux;

With palladium 10% on activated carbon; hydrogen; triethylamine; In methanol; ethyl acetate; for 48h; under 760.051 Torr;
DOI:10.1021/ol901765f

Reference yield:

: 1187663-04-2
C₁₉H₃₂O₄

: 1187663-05-3
diethyl 5-[3-(benzyloxy)propyl]nonanedioate

Guidance literature:: Multi-step reaction with 2 steps

1.1: Jones reagent / acetone

2.1: sulfuric acid / 12 h / Reflux

2.2: 6 h / 20 °C / 760.05 Torr

With Jones reagent; sulfuric acid; In acetone; 1.1: Jones oxidation;
DOI:10.1002/asia.201100480