SY₆₃₄-69P₁

Base Information

Chemical Name:SY₆₃₄-69P₁
CAS No.:1269040-78-9
Molecular Formula:C₄₆H₆₅NO₁₅
Molecular Weight:872.02
Hs Code.:

Synonyms:SY₆₃₄-69P₁

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Chemical Property of SY₆₃₄-69P₁

Chemical Property:

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Technology Process of SY₆₃₄-69P₁

There total 9 articles about SY₆₃₄-69P₁ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1029600-32-5
SY₅₈₆-170.1

: 1269040-78-9
SY₆₃₄-69P₁

Guidance literature:: With hydrogen; palladium on carbon; In tetrahydrofuran; at 20 ℃; for 1.5h;

Reference yield:

: 32981-86-5,172018-16-5
10-deacetylbaccatin III

: 1269040-78-9
SY₆₃₄-69P₁

Guidance literature:: Multi-step reaction with 9 steps

1.1: triethylamine; copper dichloride / ethyl acetate; ethanol / -13 - -1.3 °C / Inert atmosphere

1.2: 0.25 h

2.1: pyridine / -20 - 5.8 °C / Inert atmosphere

2.2: -17.5 - 20 °C

3.1: lithium borohydride / ethanol; tetrahydrofuran / -12 - 15 °C / Inert atmosphere

3.2: -10.8 - -3 °C

4.1: dmap; triethylamine / Isopropyl acetate / 3 h / 35 °C / Inert atmosphere

4.2: 0.25 h / 19.7 °C

5.1: water / acetic acid / methanol / 9 h / 50 - 55 °C

6.1: trifluoroacetic acid / toluene / -15 °C

6.2: 0.25 h / 5 °C / pH > 5

7.1: dmap; pivaloyl chloride; 4-methyl-morpholine / tetrahydrofuran / 38 °C / Inert atmosphere

8.1: hydrogenchloride / tetrahydrofuran; methanol / 2 h / 2 °C / pH 1.5 - 1.9

9.1: hydrogen / palladium on carbon / tetrahydrofuran / 1.5 h / 20 °C

With 4-methyl-morpholine; pyridine; hydrogenchloride; dmap; lithium borohydride; water; hydrogen; pivaloyl chloride; triethylamine; trifluoroacetic acid; copper dichloride; palladium on carbon; acetic acid; In tetrahydrofuran; methanol; ethanol; Isopropyl acetate; ethyl acetate; toluene;

Reference yield:

: 943239-53-0
C₄₁H₆₆O₁₀Si₂

: 1269040-78-9
SY₆₃₄-69P₁

Guidance literature:: Multi-step reaction with 6 steps

1.1: dmap; triethylamine / Isopropyl acetate / 3 h / 35 °C / Inert atmosphere

1.2: 0.25 h / 19.7 °C

2.1: water / acetic acid / methanol / 9 h / 50 - 55 °C

3.1: trifluoroacetic acid / toluene / -15 °C

3.2: 0.25 h / 5 °C / pH > 5

4.1: dmap; pivaloyl chloride; 4-methyl-morpholine / tetrahydrofuran / 38 °C / Inert atmosphere

5.1: hydrogenchloride / tetrahydrofuran; methanol / 2 h / 2 °C / pH 1.5 - 1.9

6.1: hydrogen / palladium on carbon / tetrahydrofuran / 1.5 h / 20 °C

With 4-methyl-morpholine; hydrogenchloride; dmap; water; hydrogen; pivaloyl chloride; triethylamine; trifluoroacetic acid; palladium on carbon; acetic acid; In tetrahydrofuran; methanol; Isopropyl acetate; toluene;