tetra-n-butylphosphonium.tetrakis(pentafluorophenyl)borate

Base Information

Chemical Name:tetra-n-butylphosphonium.tetrakis(pentafluorophenyl)borate
CAS No.:443889-03-0
Molecular Formula:C₁₆H₃₆P*C₂₄BF₂₀
Molecular Weight:938.479
Hs Code.:

Synonyms:tetra-n-butylphosphonium.tetrakis(pentafluorophenyl)borate

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Chemical Property of tetra-n-butylphosphonium.tetrakis(pentafluorophenyl)borate

Chemical Property:

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Technology Process of tetra-n-butylphosphonium.tetrakis(pentafluorophenyl)borate

There total 4 articles about tetra-n-butylphosphonium.tetrakis(pentafluorophenyl)borate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 3115-68-2
tetrabutyl phosphonium bromide

: 143607-32-3
silver tetrakis(pentafluorophenyl)borate

: 443889-03-0
tetra-n-butylphosphonium.tetrakis(pentafluorophenyl)borate

Guidance literature:: In dichloromethane; at 25 ℃; for 0.166667h; Darkness;
DOI:10.5560/ZNB.2014-4165

Reference yield:

: 2797-28-6
lithium tetrakis(pentafluorophenyl)borate

: 3115-68-2
tetrabutyl phosphonium bromide

: 443889-03-0
tetra-n-butylphosphonium.tetrakis(pentafluorophenyl)borate

Guidance literature:: In dichloromethane; at 25 ℃; for 2h; Schlenk technique; Inert atmosphere;
DOI:10.5560/ZNB.2014-4165

Reference yield:

: 344-04-7
bromopentafluorobenzene

: 443889-03-0
tetra-n-butylphosphonium.tetrakis(pentafluorophenyl)borate

Guidance literature:: Multi-step reaction with 2 steps

1.1: n-butyllithium / hexane; diethyl ether / 1 h / -78 °C

1.2: 1 h / -78 °C

2.1: dichloromethane / 2 h / 25 °C / Schlenk technique; Inert atmosphere

With n-butyllithium; In diethyl ether; hexane; dichloromethane;
DOI:10.5560/ZNB.2014-4165