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3115-68-2

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Tetrabutylphosphonium bromide 3115-68-2 Factory PRICE IN STOCK COA CAS 3115-68-2
Cas No: 3115-68-2
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Factory Supply Tetrabutylphosphonium bromide
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1-(3-methoxypropoxy)butane
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Tetrabutyl phosphonium bromide
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Tetrabutylphosphonium bromide CAS: 3115-68-2
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USD $ 1.0-1.0 / Kilogram 1 Kilogram 2000 Metric Ton/Year Henan Sinotech Import&Export Corporation Contact Supplier
Tetrabutylphosphonium bromide
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TIANFU CHEM----Tetrabutylphosphonium bromide
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3115-68-2 Usage

Chemical Properties

Tetrabutylphosphonium bromide is WHITE TO CREAM CRYSTALLINE POWDER

Uses

Tetrabutylphosphonium bromide is a?useful synthetic reagent used in proteomics research.
InChI:InChI=1/C16H36P.BrH/c1-5-9-13-17(14-10-6-2,15-11-7-3)16-12-8-4;/h5-16H2,1-4H3;1H/q+1;/p-1

3115-68-2 Well-known Company Product Price

Brand (Code)Product description CAS number Packaging Price Detail
TCI America (T1124)  Tetrabutylphosphonium Bromide  >99.0%(T) 3115-68-2 25g 290.00CNY Detail
TCI America (T1124)  Tetrabutylphosphonium Bromide  >99.0%(T) 3115-68-2 100g 580.00CNY Detail
TCI America (T1124)  Tetrabutylphosphonium Bromide  >99.0%(T) 3115-68-2 500g 1,990.00CNY Detail
Alfa Aesar (A10868)  Tetra-n-butylphosphonium bromide, 99%    3115-68-2 25g 203.0CNY Detail
Alfa Aesar (A10868)  Tetra-n-butylphosphonium bromide, 99%    3115-68-2 100g 434.0CNY Detail
Alfa Aesar (A10868)  Tetra-n-butylphosphonium bromide, 99%    3115-68-2 500g 1523.0CNY Detail
Aldrich (189138)  Tetrabutylphosphoniumbromide  98% 3115-68-2 189138-100G 568.62CNY Detail
Aldrich (189138)  Tetrabutylphosphoniumbromide  98% 3115-68-2 189138-500G 2,024.10CNY Detail

3115-68-2SDS

SAFETY DATA SHEETS

According to Globally Harmonized System of Classification and Labelling of Chemicals (GHS) - Sixth revised edition

Version: 1.0

Creation Date: Aug 11, 2017

Revision Date: Aug 11, 2017

1.Identification

1.1 GHS Product identifier

Product name tetrabutylphosphanium,bromide

1.2 Other means of identification

Product number -
Other names tetrabutylphosphanium bromide

1.3 Recommended use of the chemical and restrictions on use

Identified uses For industry use only.
Uses advised against no data available

1.4 Supplier's details

1.5 Emergency phone number

Emergency phone number -
Service hours Monday to Friday, 9am-5pm (Standard time zone: UTC/GMT +8 hours).

More Details:3115-68-2 SDS

3115-68-2Synthetic route

1-bromo-butane
109-65-9

1-bromo-butane

tetrabutyl phosphonium bromide
3115-68-2

tetrabutyl phosphonium bromide

Conditions
ConditionsYield
With samarium(III) chloride; phosphorous In acetonitrile at 50℃; electrosynthesis;10%
1-bromo-butane
109-65-9

1-bromo-butane

n-butyl magnesium bromide
693-03-8

n-butyl magnesium bromide

tetrabutyl phosphonium bromide
3115-68-2

tetrabutyl phosphonium bromide

Conditions
ConditionsYield
With P
1-bromo-butane
109-65-9

1-bromo-butane

tributylphosphine
998-40-3

tributylphosphine

tetrabutyl phosphonium bromide
3115-68-2

tetrabutyl phosphonium bromide

tetrabutyl phosphonium bromide
3115-68-2

tetrabutyl phosphonium bromide

tetrabutylphosphonium fluoride dihydrofluoride

tetrabutylphosphonium fluoride dihydrofluoride

Conditions
ConditionsYield
With potassium hydrogen bifluoride In dichloromethane for 0.5h; Ambient temperature;100%
tetrabutyl phosphonium bromide
3115-68-2

tetrabutyl phosphonium bromide

tetra-n-butylphosphonium tetrafluoroborate

tetra-n-butylphosphonium tetrafluoroborate

Conditions
ConditionsYield
With triethyloxonium fluoroborate In dichloromethane at 20℃; for 0.5h;100%
With trimethyl phosphite; tetrafluoroboric acid at 0 - 60℃; for 15h; Inert atmosphere; neat (no solvent);94%
With sodium tetrafluoroborate In water93%
With sodium tetrafluoroborate In dichloromethane at 120℃; for 24h; Inert atmosphere; Schlenk technique; Glovebox;90%
cis-dibromobis(trimethylphosphite-κP)platinum
31299-31-7, 77519-93-8

cis-dibromobis(trimethylphosphite-κP)platinum

tetrabutyl phosphonium bromide
3115-68-2

tetrabutyl phosphonium bromide

tetrabutylphosphonium cis-dibromo(dimethylphosphonato)(trimethylphosphite)platinum(II)
1478658-04-6

tetrabutylphosphonium cis-dibromo(dimethylphosphonato)(trimethylphosphite)platinum(II)

Conditions
ConditionsYield
In acetonitrile at 70℃; for 2h;100%
2H(1+)*C6B2N6(2-)*2H2O

2H(1+)*C6B2N6(2-)*2H2O

tetrabutyl phosphonium bromide
3115-68-2

tetrabutyl phosphonium bromide

2C16H36P(1+)*C6B2N6(2-)

2C16H36P(1+)*C6B2N6(2-)

Conditions
ConditionsYield
In water99%
sodium tetrafluoroborate
13755-29-8

sodium tetrafluoroborate

tetrabutyl phosphonium bromide
3115-68-2

tetrabutyl phosphonium bromide

tetra-n-butylphosphonium tetrafluoroborate

tetra-n-butylphosphonium tetrafluoroborate

Conditions
ConditionsYield
In pentan-1-ol98.6%
tetrabutyl phosphonium bromide
3115-68-2

tetrabutyl phosphonium bromide

phenyl chloroformate
1885-14-9

phenyl chloroformate

carbonic acid dimethyl ester
616-38-6

carbonic acid dimethyl ester

bis(phenyl) carbonate
102-09-0

bis(phenyl) carbonate

Conditions
ConditionsYield
98%
methyl phenyl carbonate
13509-27-8

methyl phenyl carbonate

tetrabutyl phosphonium bromide
3115-68-2

tetrabutyl phosphonium bromide

phenyl chloroformate
1885-14-9

phenyl chloroformate

bis(phenyl) carbonate
102-09-0

bis(phenyl) carbonate

Conditions
ConditionsYield
98%
potassium trifluoromethansulfonate
2926-27-4

potassium trifluoromethansulfonate

tetrabutyl phosphonium bromide
3115-68-2

tetrabutyl phosphonium bromide

tetra-n-butylphosphonium trifluoromethanesulfonate
126991-62-6

tetra-n-butylphosphonium trifluoromethanesulfonate

Conditions
ConditionsYield
In water98%
methyl phenyl carbonate
13509-27-8

methyl phenyl carbonate

tetrabutyl phosphonium bromide
3115-68-2

tetrabutyl phosphonium bromide

benzoyl chloride
98-88-4

benzoyl chloride

benzoic acid phenyl ester
93-99-2

benzoic acid phenyl ester

Conditions
ConditionsYield
97%
triphenyl(p-tolyl)borate potassium salt

triphenyl(p-tolyl)borate potassium salt

tetrabutyl phosphonium bromide
3115-68-2

tetrabutyl phosphonium bromide

tetrabutylphosphonium triphenyl(p-tolyl)borate

tetrabutylphosphonium triphenyl(p-tolyl)borate

Conditions
ConditionsYield
In 1,2-dichloro-ethane for 1h;97%
methyl phenyl carbonate
13509-27-8

methyl phenyl carbonate

tetrabutyl phosphonium bromide
3115-68-2

tetrabutyl phosphonium bromide

chloroacetic acid ethyl ester
105-39-5

chloroacetic acid ethyl ester

phenoxyacetic acid ethyl ester
2555-49-9

phenoxyacetic acid ethyl ester

Conditions
ConditionsYield
96%
trifluorormethanesulfonic acid
1493-13-6

trifluorormethanesulfonic acid

tetrabutyl phosphonium bromide
3115-68-2

tetrabutyl phosphonium bromide

tetra-n-butylphosphonium trifluoromethanesulfonate
126991-62-6

tetra-n-butylphosphonium trifluoromethanesulfonate

Conditions
ConditionsYield
With trimethyl phosphite at 0 - 60℃; for 15h; Inert atmosphere; neat (no solvent);96%
methyl (S)-2-(benzyloxycarbonlamino)-3-(p-toluenesulfonyl)propionate
1492-52-0

methyl (S)-2-(benzyloxycarbonlamino)-3-(p-toluenesulfonyl)propionate

tetrabutyl phosphonium bromide
3115-68-2

tetrabutyl phosphonium bromide

potassium carbonate
584-08-7

potassium carbonate

thiophenol
108-98-5

thiophenol

N-benzyloxycarbonyl-S-phenyl-L-cysteine methyl ester
153277-33-9

N-benzyloxycarbonyl-S-phenyl-L-cysteine methyl ester

Conditions
ConditionsYield
In water; toluene94.6%
2-bromo-N-(4-chlorophenyl)butanamide
90841-17-1

2-bromo-N-(4-chlorophenyl)butanamide

tetrabutyl phosphonium bromide
3115-68-2

tetrabutyl phosphonium bromide

N-(4-chloro)phenyl-2-hydroxy butyramide
72468-65-6

N-(4-chloro)phenyl-2-hydroxy butyramide

Conditions
ConditionsYield
With sodium hydroxide; sodium formate In water; toluene94%
bis[bis(pentafluoroethyl)phosphinyl]imide
916079-45-3

bis[bis(pentafluoroethyl)phosphinyl]imide

tetrabutyl phosphonium bromide
3115-68-2

tetrabutyl phosphonium bromide

tetra(n-butyl)phosphonium bis[bis(pentafluoroethyl)phosphinyl]azanide

tetra(n-butyl)phosphonium bis[bis(pentafluoroethyl)phosphinyl]azanide

Conditions
ConditionsYield
In water at 20℃;94%
In water at 20℃;86%
ethene
74-85-1

ethene

tetrabutyl phosphonium bromide
3115-68-2

tetrabutyl phosphonium bromide

platinum(II) bromde

platinum(II) bromde

[nBu4P][PtBr3(C2H4)]
1184173-10-1

[nBu4P][PtBr3(C2H4)]

Conditions
ConditionsYield
In toluene at 150℃; under 18751.9 Torr; for 15h; Autoclave;94%
In toluene pptd. (Et2O);
sodium tungstate (VI) dihydrate
10213-10-2

sodium tungstate (VI) dihydrate

tetraoxo-μ-oxobis(pentamethylcyclopentadienyl)ditungsten(VI)

tetraoxo-μ-oxobis(pentamethylcyclopentadienyl)ditungsten(VI)

tetrabutyl phosphonium bromide
3115-68-2

tetrabutyl phosphonium bromide

P(C4H9)4(1+)*(C5(CH3)5)W6O18(1-)=P(C4H9)4(C5(CH3)5)W6O18

P(C4H9)4(1+)*(C5(CH3)5)W6O18(1-)=P(C4H9)4(C5(CH3)5)W6O18

Conditions
ConditionsYield
With HNO3 In methanol; water byproducts: H2O; (C5(CH3)5)W2O5 in methanol was mixed with an aq. soln. of Na2WO4*2H2O, aq. HNO3 was added, stirring for 2 h, bromide salt in water was added; ppt. was filtered off, washed with small portions of water, methanol anddiethyl ether, dried under vac. at 70°C; elem. anal.;94%
propyl methanesulfonate
1912-31-8

propyl methanesulfonate

tetrabutyl phosphonium bromide
3115-68-2

tetrabutyl phosphonium bromide

A

propyl bromide
106-94-5

propyl bromide

B

tetrabutylphosphonium methanesulfonate
98342-59-7

tetrabutylphosphonium methanesulfonate

Conditions
ConditionsYield
In benzene at 80℃;A n/a
B 93%
tetrabutyl phosphonium bromide
3115-68-2

tetrabutyl phosphonium bromide

2-methylsulfanyl-6,7,8,9-tetrahydro-1,2,4-triazolo[5,1-b]quinazoline-5(10H)-one
124005-47-6

2-methylsulfanyl-6,7,8,9-tetrahydro-1,2,4-triazolo[5,1-b]quinazoline-5(10H)-one

2-methylthio-6,7,8,9-tetrahydro-1,2,4-triazolo[5,1-b]quinazolin-5(10H)-one tetrabutylphosphonium salt

2-methylthio-6,7,8,9-tetrahydro-1,2,4-triazolo[5,1-b]quinazolin-5(10H)-one tetrabutylphosphonium salt

Conditions
ConditionsYield
With sodium hydroxide In chloroform at 20℃; for 0.0833333h;93%
potassium hexabromoplatinate(IV)

potassium hexabromoplatinate(IV)

tetrabutyl phosphonium bromide
3115-68-2

tetrabutyl phosphonium bromide

tetrabutylphosphonium hexabromoplatinate

tetrabutylphosphonium hexabromoplatinate

Conditions
ConditionsYield
In acetone93%
gold-colored oil

gold-colored oil

1-butanethiol
109-79-5

1-butanethiol

ethylphosphonothioic dichloride
993-43-1

ethylphosphonothioic dichloride

tetrabutyl phosphonium bromide
3115-68-2

tetrabutyl phosphonium bromide

S-n-butyl ethylphosphonodithioic chloride
17162-58-2

S-n-butyl ethylphosphonodithioic chloride

Conditions
ConditionsYield
With sodium carbonate In diethyl ether92.5%
sodium molybdate dihydrate
7631-95-0

sodium molybdate dihydrate

tetraoxo-μ-oxobis(pentamethylcyclopentadienyl)dimolybdenum(VI)

tetraoxo-μ-oxobis(pentamethylcyclopentadienyl)dimolybdenum(VI)

tetrabutyl phosphonium bromide
3115-68-2

tetrabutyl phosphonium bromide

P(C4H9)4(1+)*(C5(CH3)5)Mo6O18(1-)=P(C4H9)4(C5(CH3)5)Mo6O18

P(C4H9)4(1+)*(C5(CH3)5)Mo6O18(1-)=P(C4H9)4(C5(CH3)5)Mo6O18

Conditions
ConditionsYield
With HNO3 In methanol; water byproducts: H2O; (C5(CH3)5)Mo2O5 in methanol was mixed with an aq. soln. of Na2MoO4*2H2O,aq. HNO3 was added, stirring for 2 h, bromide salt in water was added; ppt. was filtered off, washed with small portions of water, methanol anddiethyl ether, dried under vac. at 70°C; elem. anal.;92%
silver(I) tungstate

silver(I) tungstate

tetrabutyl phosphonium bromide
3115-68-2

tetrabutyl phosphonium bromide

2C16H36P(1+)*O4W(2-)

2C16H36P(1+)*O4W(2-)

Conditions
ConditionsYield
In water for 0.166667h;92%
potassium tetracyanoborate

potassium tetracyanoborate

tetrabutyl phosphonium bromide
3115-68-2

tetrabutyl phosphonium bromide

tetra-n-butylphosphonium tetracyanidoborate
916730-42-2

tetra-n-butylphosphonium tetracyanidoborate

Conditions
ConditionsYield
In acetonitrile for 0.25h;91%
In acetonitrile byproducts: KBr; solns. of K(B(CN)4) (1.624 mmol) and P(C4H9)4Br mixed, stireed for 15 min; centrifuged, solvent evapd., ppt. washed (Et2O), dried at room temp. (under vac.), recrystd. from CH3CN; elem. anal.;91%
sodium metavanadate

sodium metavanadate

tetrabutyl phosphonium bromide
3115-68-2

tetrabutyl phosphonium bromide

[tris(tetrabutylphosphonium)] decavanadateH3

[tris(tetrabutylphosphonium)] decavanadateH3

Conditions
ConditionsYield
With nitric acid In water for 0.0833333h; pH=4.5;91%
silver(I) tetrakis(3,5-bis(trifluoromethyl)phenyl)borate
160298-76-0

silver(I) tetrakis(3,5-bis(trifluoromethyl)phenyl)borate

tetrabutyl phosphonium bromide
3115-68-2

tetrabutyl phosphonium bromide

C16H36P(1+)*C32H12BF24(1-)

C16H36P(1+)*C32H12BF24(1-)

Conditions
ConditionsYield
In dichloromethane at 25℃; for 0.166667h; Darkness; Schlenk technique;91%
tetrabutyl phosphonium bromide
3115-68-2

tetrabutyl phosphonium bromide

tetrabutylphosphonium nitrate

tetrabutylphosphonium nitrate

Conditions
ConditionsYield
With trimethyl phosphite; nitric acid at 0 - 60℃; for 15h; Inert atmosphere; neat (no solvent);90%
tetrabutyl phosphonium bromide
3115-68-2

tetrabutyl phosphonium bromide

bis(trifluoromethane)sulfonimide lithium
90076-65-6

bis(trifluoromethane)sulfonimide lithium

tetrabutylphosphonium bis(trifluoromethanesulfonyl)amide

tetrabutylphosphonium bis(trifluoromethanesulfonyl)amide

Conditions
ConditionsYield
In dichloromethane at 120℃; for 24h; Inert atmosphere; Schlenk technique; Glovebox;90%
In water for 2h;
K[cis-PF2(CN)4]

K[cis-PF2(CN)4]

tetrabutyl phosphonium bromide
3115-68-2

tetrabutyl phosphonium bromide

[(n-Bu4)P][cis-PF2(CN)4]

[(n-Bu4)P][cis-PF2(CN)4]

Conditions
ConditionsYield
In dichloromethane; water at 20℃; for 1h;90%
phosphoric acid O,O'-bis-(3-pentadecyl-phenyl) ester

phosphoric acid O,O'-bis-(3-pentadecyl-phenyl) ester

tetrabutyl phosphonium bromide
3115-68-2

tetrabutyl phosphonium bromide

C42H70O4P(1-)*C16H36P(1+)

C42H70O4P(1-)*C16H36P(1+)

Conditions
ConditionsYield
With potassium hydroxide In hexane; water at 20℃; for 6h;90%
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