2-[2,4,6-tris[bis(trimethylsilyl)methyl]phenyl]-2-(2,4,6-tricyclohexylphenyl)-4-mesityl-1,3,5,2-oxathiazastannole

Base Information

Chemical Name:2-[2,4,6-tris[bis(trimethylsilyl)methyl]phenyl]-2-(2,4,6-tricyclohexylphenyl)-4-mesityl-1,3,5,2-oxathiazastannole
CAS No.:820217-31-0
Molecular Formula:C₆₁H₁₀₅NOSSi₆Sn
Molecular Weight:1187.8
Hs Code.:

Synonyms:2-[2,4,6-tris[bis(trimethylsilyl)methyl]phenyl]-2-(2,4,6-tricyclohexylphenyl)-4-mesityl-1,3,5,2-oxathiazastannole

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Chemical Property of 2-[2,4,6-tris[bis(trimethylsilyl)methyl]phenyl]-2-(2,4,6-tricyclohexylphenyl)-4-mesityl-1,3,5,2-oxathiazastannole

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Technology Process of 2-[2,4,6-tris[bis(trimethylsilyl)methyl]phenyl]-2-(2,4,6-tricyclohexylphenyl)-4-mesityl-1,3,5,2-oxathiazastannole

There total 6 articles about 2-[2,4,6-tris[bis(trimethylsilyl)methyl]phenyl]-2-(2,4,6-tricyclohexylphenyl)-4-mesityl-1,3,5,2-oxathiazastannole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 35.0%

: 176763-10-3
5-(2,4,6-tricyclohexylphenyl)-5-[2,4,6-tris[bis(trimethylsilyl)methyl]phenyl]-1,2,3,4,5-tetrathiastannolane

: 2904-57-6
mesitylenecarbonitrile oxide

: 820217-31-0
2-[2,4,6-tris[bis(trimethylsilyl)methyl]phenyl]-2-(2,4,6-tricyclohexylphenyl)-4-mesityl-1,3,5,2-oxathiazastannole

Guidance literature:: With PPh₃; In hexane; byproducts: Ph3P=S; (Ar); hexane added to a mixt. of PPh3 and Sn compd., degassed, sealed, kept at room temp. overnight, poured into mesitonitrile oxide; solvent-removed, subjected to HPLC, recrystd. (CH2Cl2/MeCN); elem. anal.;
DOI:10.1021/ja048453h

Reference yield:

: 97443-80-6
(2-bromobenzene-1,3,5-triyl)tricyclohexane

: 820217-31-0
2-[2,4,6-tris[bis(trimethylsilyl)methyl]phenyl]-2-(2,4,6-tricyclohexylphenyl)-4-mesityl-1,3,5,2-oxathiazastannole

Guidance literature:: Multi-step reaction with 5 steps

1: t-BuLi; Mg; I₂ / pentane; tetrahydrofuran

2: LiAlH₄ / tetrahydrofuran

3: diethyl ether

4: lithium naphthalenide / tetrahydrofuran

5: PPh₃ / hexane

With t-BuLi; Mg; I₂; LiAlH₄; lithium naphthalenide; PPh₃; In tetrahydrofuran; diethyl ether; hexane; pentane;
DOI:10.1021/ja048453h

Reference yield:

: 820217-14-9
dibromo(2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)(2,4,6-tricyclohexylphenyl)stannane

: 820217-31-0
2-[2,4,6-tris[bis(trimethylsilyl)methyl]phenyl]-2-(2,4,6-tricyclohexylphenyl)-4-mesityl-1,3,5,2-oxathiazastannole

Guidance literature:: Multi-step reaction with 2 steps

1: lithium naphthalenide / tetrahydrofuran

2: PPh₃ / hexane

With lithium naphthalenide; PPh₃; In tetrahydrofuran; hexane;
DOI:10.1021/ja048453h