{2-[2-(2-{[(2R,3R,4S,5R,6R)-3,4-Diacetoxy-6-acetoxymethyl-5-((2S,3R,4S,5S,6R)-3,4,5-triacetoxy-6-acetoxymethyl-tetrahydro-pyran-2-yloxy)-tetrahydro-pyran-2-ylcarbamoyl]-methoxy}-ethoxy)-ethoxy]-ethylamino}-acetic acid tert-butyl ester

Base Information

Chemical Name:{2-[2-(2-{[(2R,3R,4S,5R,6R)-3,4-Diacetoxy-6-acetoxymethyl-5-((2S,3R,4S,5S,6R)-3,4,5-triacetoxy-6-acetoxymethyl-tetrahydro-pyran-2-yloxy)-tetrahydro-pyran-2-ylcarbamoyl]-methoxy}-ethoxy)-ethoxy]-ethylamino}-acetic acid tert-butyl ester
CAS No.:176167-87-6
Molecular Formula:C₄₀H₆₂N₂O₂₃
Molecular Weight:938.932
Hs Code.:

{2-[2-(2-{[(2R,3R,4S,5R,6R)-3,4-Diacetoxy-6-acetoxymethyl-5-((2S,3R,4S,5S,6R)-3,4,5-triacetoxy-6-acetoxymethyl-tetrahydro-pyran-2-yloxy)-tetrahydro-pyran-2-ylcarbamoyl]-methoxy}-ethoxy)-ethoxy]-ethylamino}-acetic acid tert-butyl ester

Synonyms:{2-[2-(2-{[(2R,3R,4S,5R,6R)-3,4-Diacetoxy-6-acetoxymethyl-5-((2S,3R,4S,5S,6R)-3,4,5-triacetoxy-6-acetoxymethyl-tetrahydro-pyran-2-yloxy)-tetrahydro-pyran-2-ylcarbamoyl]-methoxy}-ethoxy)-ethoxy]-ethylamino}-acetic acid tert-butyl ester

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Chemical Property of {2-[2-(2-{[(2R,3R,4S,5R,6R)-3,4-Diacetoxy-6-acetoxymethyl-5-((2S,3R,4S,5S,6R)-3,4,5-triacetoxy-6-acetoxymethyl-tetrahydro-pyran-2-yloxy)-tetrahydro-pyran-2-ylcarbamoyl]-methoxy}-ethoxy)-ethoxy]-ethylamino}-acetic acid tert-butyl ester

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Technology Process of {2-[2-(2-{[(2R,3R,4S,5R,6R)-3,4-Diacetoxy-6-acetoxymethyl-5-((2S,3R,4S,5S,6R)-3,4,5-triacetoxy-6-acetoxymethyl-tetrahydro-pyran-2-yloxy)-tetrahydro-pyran-2-ylcarbamoyl]-methoxy}-ethoxy)-ethoxy]-ethylamino}-acetic acid tert-butyl ester

There total 1 articles about {2-[2-(2-{[(2R,3R,4S,5R,6R)-3,4-Diacetoxy-6-acetoxymethyl-5-((2S,3R,4S,5S,6R)-3,4,5-triacetoxy-6-acetoxymethyl-tetrahydro-pyran-2-yloxy)-tetrahydro-pyran-2-ylcarbamoyl]-methoxy}-ethoxy)-ethoxy]-ethylamino}-acetic acid tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 86520-52-7
2-[2-(2-azidoethoxy)ethoxy]ethanol

: 176167-87-6
{2-[2-(2-{[(2R,3R,4S,5R,6R)-3,4-Diacetoxy-6-acetoxymethyl-5-((2S,3R,4S,5S,6R)-3,4,5-triacetoxy-6-acetoxymethyl-tetrahydro-pyran-2-yloxy)-tetrahydro-pyran-2-ylcarbamoyl]-methoxy}-ethoxy)-ethoxy]-ethylamino}-acetic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: 80 percent / BF₃*Et₂O / CH₂Cl₂ / 6 h / Ambient temperature

2: aq. KOH / ethanol / 6 h / Heating

3: 90 percent / DCC / CH₂Cl₂ / 1 h / Ambient temperature

4: H₂ / 10percent Pd/C / methanol / 1 h

5: 65 percent / DIPEA / acetonitrile / 3 h / Ambient temperature

With potassium hydroxide; boron trifluoride diethyl etherate; hydrogen; N-ethyl-N,N-diisopropylamine; dicyclohexyl-carbodiimide; palladium on activated charcoal; In methanol; ethanol; dichloromethane; acetonitrile;
DOI:10.1039/cc9960000201

Reference yield: 85.0%

: 1138-80-3
N-(Benzyloxycarbonyl)glycine

: 176167-87-6
{2-[2-(2-{[(2R,3R,4S,5R,6R)-3,4-Diacetoxy-6-acetoxymethyl-5-((2S,3R,4S,5S,6R)-3,4,5-triacetoxy-6-acetoxymethyl-tetrahydro-pyran-2-yloxy)-tetrahydro-pyran-2-ylcarbamoyl]-methoxy}-ethoxy)-ethoxy]-ethylamino}-acetic acid tert-butyl ester

: 176167-88-7
C₅₀H₇₁N₃O₂₆

Guidance literature:: With dicyclohexyl-carbodiimide; In dichloromethane; for 3h; Ambient temperature;
DOI:10.1039/cc9960000201

Reference yield:

: 176167-87-6
{2-[2-(2-{[(2R,3R,4S,5R,6R)-3,4-Diacetoxy-6-acetoxymethyl-5-((2S,3R,4S,5S,6R)-3,4,5-triacetoxy-6-acetoxymethyl-tetrahydro-pyran-2-yloxy)-tetrahydro-pyran-2-ylcarbamoyl]-methoxy}-ethoxy)-ethoxy]-ethylamino}-acetic acid tert-butyl ester

: 176167-91-2
C₄₆H₆₃N₃O₂₆

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / DCC / CH₂Cl₂ / 3 h / Ambient temperature

2: 94 percent / TFA / CH₂Cl₂ / 3 h / Ambient temperature

With dicyclohexyl-carbodiimide; trifluoroacetic acid; In dichloromethane;
DOI:10.1039/cc9960000201