7-(2-azidophenyl)-8-methoxy-5-phenylquinoline

Base Information

Chemical Name:7-(2-azidophenyl)-8-methoxy-5-phenylquinoline
CAS No.:172795-94-7
Molecular Formula:C₂₂H₁₆N₄O
Molecular Weight:352.395
Hs Code.:

Synonyms:7-(2-azidophenyl)-8-methoxy-5-phenylquinoline

Suppliers and Price of 7-(2-azidophenyl)-8-methoxy-5-phenylquinoline

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Chemical Property of 7-(2-azidophenyl)-8-methoxy-5-phenylquinoline

Chemical Property:

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Technology Process of 7-(2-azidophenyl)-8-methoxy-5-phenylquinoline

There total 5 articles about 7-(2-azidophenyl)-8-methoxy-5-phenylquinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 17012-49-6
5,7-dibromo-8-methoxyquinoline

: 172795-94-7
7-(2-azidophenyl)-8-methoxy-5-phenylquinoline

Guidance literature:: Multi-step reaction with 4 steps

1: 94 percent / sodium carbonate / tetrakis(triphenylphosphine)palladium⁽⁰⁾ / methanol; toluene / 72 h / Heating

2: 57 percent / potassium carbonate / tetrakis(triphenylphosphine)palladium⁽⁰⁾ / ethanol; toluene / 72 h / Heating

3: 91 percent / 20percent sulfuric acid / 6 h / Heating

4: 1.) conc. sulfuric acid, sodium nitrite; 2.) sodium azide / 1.) water, 45 min; 2.) water, 40 min

With sodium azide; sulfuric acid; sodium carbonate; potassium carbonate; sodium nitrite; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In methanol; ethanol; toluene;
DOI:10.1016/0040-4020(95)00726-O

Reference yield:

: 170959-58-7
7-bromo-5-phenyl-8-methoxyquinoline

: 172795-94-7
7-(2-azidophenyl)-8-methoxy-5-phenylquinoline

Guidance literature:: Multi-step reaction with 3 steps

1: 57 percent / potassium carbonate / tetrakis(triphenylphosphine)palladium⁽⁰⁾ / ethanol; toluene / 72 h / Heating

2: 91 percent / 20percent sulfuric acid / 6 h / Heating

3: 1.) conc. sulfuric acid, sodium nitrite; 2.) sodium azide / 1.) water, 45 min; 2.) water, 40 min

With sodium azide; sulfuric acid; potassium carbonate; sodium nitrite; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In ethanol; toluene;
DOI:10.1016/0040-4020(95)00726-O

Reference yield:

: 98-80-6
phenylboronic acid

: 172795-94-7
7-(2-azidophenyl)-8-methoxy-5-phenylquinoline

Guidance literature:: Multi-step reaction with 4 steps

1: 94 percent / sodium carbonate / tetrakis(triphenylphosphine)palladium⁽⁰⁾ / methanol; toluene / 72 h / Heating

2: 57 percent / potassium carbonate / tetrakis(triphenylphosphine)palladium⁽⁰⁾ / ethanol; toluene / 72 h / Heating

3: 91 percent / 20percent sulfuric acid / 6 h / Heating

4: 1.) conc. sulfuric acid, sodium nitrite; 2.) sodium azide / 1.) water, 45 min; 2.) water, 40 min

With sodium azide; sulfuric acid; sodium carbonate; potassium carbonate; sodium nitrite; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In methanol; ethanol; toluene;
DOI:10.1016/0040-4020(95)00726-O