(E)-S-4-((4-((4-(trifluoromethyl)phenyl)diazenyl)phenyl)ethynyl)phenyl ethanethioate

Base Information

Chemical Name:(E)-S-4-((4-((4-(trifluoromethyl)phenyl)diazenyl)phenyl)ethynyl)phenyl ethanethioate
CAS No.:915721-78-7
Molecular Formula:C₂₃H₁₅F₃N₂OS
Molecular Weight:424.446
Hs Code.:

Synonyms:(E)-S-4-((4-((4-(trifluoromethyl)phenyl)diazenyl)phenyl)ethynyl)phenyl ethanethioate

Suppliers and Price of (E)-S-4-((4-((4-(trifluoromethyl)phenyl)diazenyl)phenyl)ethynyl)phenyl ethanethioate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-S-4-((4-((4-(trifluoromethyl)phenyl)diazenyl)phenyl)ethynyl)phenyl ethanethioate

Chemical Property:

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Technology Process of (E)-S-4-((4-((4-(trifluoromethyl)phenyl)diazenyl)phenyl)ethynyl)phenyl ethanethioate

There total 3 articles about (E)-S-4-((4-((4-(trifluoromethyl)phenyl)diazenyl)phenyl)ethynyl)phenyl ethanethioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 915721-94-7
(E)-1-(4-iodophenyl)-2-(4-(trifluoromethyl)phenyl)diazene

: 170159-24-7
acetylsulfanyl-4-(ethynyl)benzene

: 915721-78-7
(E)-S-4-((4-((4-(trifluoromethyl)phenyl)diazenyl)phenyl)ethynyl)phenyl ethanethioate

Guidance literature:: With triethylamine; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; In tetrahydrofuran;
DOI:10.1016/j.tet.2006.08.069

Reference yield:

: 455-14-1
4-trifluoromethylphenylamine

: 915721-78-7
(E)-S-4-((4-((4-(trifluoromethyl)phenyl)diazenyl)phenyl)ethynyl)phenyl ethanethioate

Guidance literature:: Multi-step reaction with 3 steps

1: Oxone(R) / CH₂Cl₂; H₂O / 20 °C

2: 1.40 g / acetic acid / 20 °C

3: 71 percent / triethylamine / bis(triphenylphosphine)palladium(II) dichloride; copper(I) iodide / tetrahydrofuran

With oxone; triethylamine; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; In tetrahydrofuran; dichloromethane; water; acetic acid;
DOI:10.1016/j.tet.2006.08.069

Reference yield:

: 34913-26-3
4-nitroso-1-(trifluoromethyl)benzene

: 915721-78-7
(E)-S-4-((4-((4-(trifluoromethyl)phenyl)diazenyl)phenyl)ethynyl)phenyl ethanethioate

Guidance literature:: Multi-step reaction with 2 steps

1: 1.40 g / acetic acid / 20 °C

2: 71 percent / triethylamine / bis(triphenylphosphine)palladium(II) dichloride; copper(I) iodide / tetrahydrofuran

With triethylamine; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; In tetrahydrofuran; acetic acid;
DOI:10.1016/j.tet.2006.08.069