C₁₆H₁₈FN₅O₂S

Base Information

Chemical Name:C₁₆H₁₈FN₅O₂S
CAS No.:1248501-48-5
Molecular Formula:C₁₆H₁₈FN₅O₂S
Molecular Weight:363.416
Hs Code.:

C<sub>16</sub>H<sub>18</sub>FN<sub>5</sub>O<sub>2</sub>S

Synonyms:C₁₆H₁₈FN₅O₂S

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Chemical Property of C₁₆H₁₈FN₅O₂S

Chemical Property:

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Technology Process of C₁₆H₁₈FN₅O₂S

There total 11 articles about C₁₆H₁₈FN₅O₂S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1248504-07-5
C₁₀H₁₄FN₃S

: 40155-42-8
5-methoxy-pyrazine-2-carboxylic acid

: 1248501-48-5
C₁₆H₁₈FN₅O₂S

Guidance literature:: C₁₀H₁₄FN₃S; 5-methoxy-pyrazine-2-carboxylic acid; With hydrogenchloride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In methanol; water; at 20 ℃; for 1h;

With sodium hydrogencarbonate; In methanol; water; ethyl acetate;

Reference yield:

: 79110-05-7
1-(2-fluoro-5-nitrophenyl)ethanone

: 1248501-48-5
C₁₆H₁₈FN₅O₂S

Guidance literature:: Multi-step reaction with 11 steps

1: water; ammonium chloride; iron / ethanol; tetrahydrofuran / 2 h / 20 - 70 °C

2: dmap; triethylamine / dichloromethane / 20 °C

3: sodium tetrahydroborate / dichloromethane; methanol / 0.5 h / cooling with ice

4: triethylamine / dichloromethane / 1.5 h / 20 °C

5: sodium azide / N,N-dimethyl-formamide / 1 h / 90 °C

6: triphenylphosphine / tetrahydrofuran / 4 h / 50 - 70 °C

7: tetrahydrofuran / 0.5 h / 20 °C

8: sodium hydroxide; water / methanol / 0.42 h / 50 °C

9: acetonitrile / 3 h / 60 °C

10: trifluoroacetic acid / chloroform / 1.33 h / 20 °C

11: hydrogenchloride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / water; methanol / 1 h / 20 °C

With hydrogenchloride; dmap; sodium tetrahydroborate; sodium azide; water; iron; ammonium chloride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; triphenylphosphine; trifluoroacetic acid; sodium hydroxide; In tetrahydrofuran; methanol; ethanol; dichloromethane; chloroform; water; N,N-dimethyl-formamide; acetonitrile;

Reference yield:

: 386216-31-5
(3-acetyl-4-fluorophenyl)carbamic acid tert-butyl ester

: 1248501-48-5
C₁₆H₁₈FN₅O₂S

Guidance literature:: Multi-step reaction with 9 steps

1: sodium tetrahydroborate / dichloromethane; methanol / 0.5 h / cooling with ice

2: triethylamine / dichloromethane / 1.5 h / 20 °C

3: sodium azide / N,N-dimethyl-formamide / 1 h / 90 °C

4: triphenylphosphine / tetrahydrofuran / 4 h / 50 - 70 °C

5: tetrahydrofuran / 0.5 h / 20 °C

6: sodium hydroxide; water / methanol / 0.42 h / 50 °C

7: acetonitrile / 3 h / 60 °C

8: trifluoroacetic acid / chloroform / 1.33 h / 20 °C

9: hydrogenchloride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / water; methanol / 1 h / 20 °C

With hydrogenchloride; sodium tetrahydroborate; sodium azide; water; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; triphenylphosphine; trifluoroacetic acid; sodium hydroxide; In tetrahydrofuran; methanol; dichloromethane; chloroform; water; N,N-dimethyl-formamide; acetonitrile;