(1R,4'S)-N-tert-butoxycarbonyl-1-(2',2'-dimethyl-[1',3']-dioxolan-4'-yl)-3-phenylpropylamine

Base Information

Chemical Name:(1R,4'S)-N-tert-butoxycarbonyl-1-(2',2'-dimethyl-[1',3']-dioxolan-4'-yl)-3-phenylpropylamine
CAS No.:872728-70-6
Molecular Formula:C₁₉H₂₉NO₄
Molecular Weight:335.444
Hs Code.:

Synonyms:(1R,4'S)-N-tert-butoxycarbonyl-1-(2',2'-dimethyl-[1',3']-dioxolan-4'-yl)-3-phenylpropylamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1R,4'S)-N-tert-butoxycarbonyl-1-(2',2'-dimethyl-[1',3']-dioxolan-4'-yl)-3-phenylpropylamine

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Technology Process of (1R,4'S)-N-tert-butoxycarbonyl-1-(2',2'-dimethyl-[1',3']-dioxolan-4'-yl)-3-phenylpropylamine

There total 8 articles about (1R,4'S)-N-tert-butoxycarbonyl-1-(2',2'-dimethyl-[1',3']-dioxolan-4'-yl)-3-phenylpropylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 872728-72-8
N-tert-butoxycarbonyl-1-(2',2'-dimethyl-[1',3']-dioxolan-4'-yl)-3-phenyl-2-(phenylsulfonyl)propylamine

: (S)-2,2-Dimethyl-4-((E)-3-phenyl-propenyl)-[1,3]dioxolane

: 872728-70-6
(1R,4'S)-N-tert-butoxycarbonyl-1-(2',2'-dimethyl-[1',3']-dioxolan-4'-yl)-3-phenylpropylamine

Guidance literature:: With sodium amalgam; In methanol; at 20 ℃; for 1h;
DOI:10.1016/j.tet.2005.09.046

Reference yield: 65.0%

: 872728-80-8
N-tert-butoxycarbonyl-1-(2',2'-dimethyl-[1',3']-dioxolan-4'-yl)-3-phenyl-2-(phenylsulfonyl)propylamine

: (S)-2,2-Dimethyl-4-((E)-3-phenyl-propenyl)-[1,3]dioxolane

: 872728-70-6
(1R,4'S)-N-tert-butoxycarbonyl-1-(2',2'-dimethyl-[1',3']-dioxolan-4'-yl)-3-phenylpropylamine

Guidance literature:: With sodium amalgam; In methanol; at 20 ℃; for 0.5h;
DOI:10.1016/j.tet.2005.09.046

Reference yield: 48.0%

: 872728-67-1
Benzyl-[(E)-(R)-1-((S)-2,2-dimethyl-[1,3]dioxolan-4-yl)-3-phenyl-allyl]-amine

: 24424-99-5
di-tert-butyl dicarbonate

: (S)-2,2-Dimethyl-4-((E)-3-phenyl-propenyl)-[1,3]dioxolane

: 872728-70-6
(1R,4'S)-N-tert-butoxycarbonyl-1-(2',2'-dimethyl-[1',3']-dioxolan-4'-yl)-3-phenylpropylamine

Guidance literature:: With hydrogen; palladium dihydroxide; In ethyl acetate; at 20 ℃; for 24h; atmospheric pressure;
DOI:10.1016/j.tet.2005.09.046