(S)-3-(tert-butyldimethylsilyloxy)-5-(4-methoxybenzyloxy)-4,4-dimethylpentanoic acid

Base Information

Chemical Name:(S)-3-(tert-butyldimethylsilyloxy)-5-(4-methoxybenzyloxy)-4,4-dimethylpentanoic acid
CAS No.:1414941-23-3
Molecular Formula:C₂₁H₃₆O₅Si
Molecular Weight:396.599
Hs Code.:

Synonyms:(S)-3-(tert-butyldimethylsilyloxy)-5-(4-methoxybenzyloxy)-4,4-dimethylpentanoic acid

Suppliers and Price of (S)-3-(tert-butyldimethylsilyloxy)-5-(4-methoxybenzyloxy)-4,4-dimethylpentanoic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (S)-3-(tert-butyldimethylsilyloxy)-5-(4-methoxybenzyloxy)-4,4-dimethylpentanoic acid

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (S)-3-(tert-butyldimethylsilyloxy)-5-(4-methoxybenzyloxy)-4,4-dimethylpentanoic acid

There total 8 articles about (S)-3-(tert-butyldimethylsilyloxy)-5-(4-methoxybenzyloxy)-4,4-dimethylpentanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 1414941-33-5
methyl 2-(2-(4-methoxybenzyloxy)ethyl)oxazole-4-carboxylate

: 1414941-23-3
(S)-3-(tert-butyldimethylsilyloxy)-5-(4-methoxybenzyloxy)-4,4-dimethylpentanoic acid

Guidance literature:: With sodium dihydrogenphosphate; 2-methyl-but-2-ene; sodium chlorite; In water; tert-butyl alcohol; at 20 ℃; for 1.5h; Inert atmosphere;
DOI:10.1021/jo302134y

Reference yield:

: 1414941-22-2
(S)-tert-butyl(1-(4-methoxybenzyloxy)-2,2-dimethylhex-5-en-3-yloxy)dimethylsilane

: 1414941-23-3
(S)-3-(tert-butyldimethylsilyloxy)-5-(4-methoxybenzyloxy)-4,4-dimethylpentanoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: ozone; triphenylphosphine; oxygen / dichloromethane / -78 - 20 °C

2: 2-methyl-but-2-ene; sodium dihydrogenphosphate; sodium chlorite / tert-butyl alcohol; water / 1.5 h / 20 °C / Inert atmosphere

With sodium dihydrogenphosphate; 2-methyl-but-2-ene; sodium chlorite; oxygen; ozone; triphenylphosphine; In dichloromethane; water; tert-butyl alcohol;
DOI:10.1021/jo302134y

Reference yield:

: 885674-86-2
(S)-1-(4-methoxybenzyloxy)-2,2-dimethylhex-5-en-3-ol

: 1414941-23-3
(S)-3-(tert-butyldimethylsilyloxy)-5-(4-methoxybenzyloxy)-4,4-dimethylpentanoic acid

Guidance literature:: Multi-step reaction with 3 steps

1: Inert atmosphere

2: ozone; triphenylphosphine; oxygen / dichloromethane / -78 - 20 °C

3: 2-methyl-but-2-ene; sodium dihydrogenphosphate; sodium chlorite / tert-butyl alcohol; water / 1.5 h / 20 °C / Inert atmosphere

With sodium dihydrogenphosphate; 2-methyl-but-2-ene; sodium chlorite; oxygen; ozone; triphenylphosphine; In dichloromethane; water; tert-butyl alcohol;
DOI:10.1021/jo302134y