2-methoxybenzyl methyl carbonate

Base Information

• Chemical Name: 2-methoxybenzyl methyl carbonate
• CAS No.: 1216910-25-6
• Molecular Formula: C₁₀H₁₂O₄
• Molecular Weight: 196.203

Synonyms:2-methoxybenzyl methyl carbonate

Chemical Property of 2-methoxybenzyl methyl carbonate

Chemical Property:

Purity/Quality:

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Technology Process of 2-methoxybenzyl methyl carbonate

There total 1 articles about 2-methoxybenzyl methyl carbonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(2-methoxyphenyl)methanol (612-16-8) + methyl chloroformate (79-22-1) → 2-methoxybenzyl methyl carbonate (1216910-25-6)

Guidance literature:

With tetra(n-butyl)ammonium hydrogensulfate; sodium hydroxide; In dichloromethane; water; at 0 - 20 ℃; Inert atmosphere;

DOI:10.1021/0l1002576

Reference yield: 92.0%

benzoxazole (273-53-0,29791-96-6) + 2-methoxybenzyl methyl carbonate (1216910-25-6) → 2-(2-methoxybenzyl)benzoxazole (1159517-77-7)

Guidance literature:

With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; 1,3-bis-(diphenylphosphino)propane; sodium acetate; In dimethyl sulfoxide; at 120 ℃; for 3h; Inert atmosphere;

DOI:10.1021/0l1002576

Reference yield: 79.0%

2-phenyl-1,3,4-oxadiazole (825-56-9) + 2-methoxybenzyl methyl carbonate (1216910-25-6) → 2-(2-methoxybenzyl)-5-phenyl-1,3,4-oxadiazole (1216910-68-7)

Guidance literature:

With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; 1,3-bis-(diphenylphosphino)propane; sodium acetate; In dimethyl sulfoxide; at 120 ℃; for 3h; Inert atmosphere;

DOI:10.1021/0l1002576

upstream raw materials:

(2-methoxyphenyl)methanol

methyl chloroformate

Downstream raw materials:

2-(2-methoxybenzyl)benzoxazole

2-(2-methoxybenzyl)-5-phenyl-1,3,4-oxadiazole

2-[2-(2-methoxyphenyl)-1-phenylethyl]benzoxazole

methanol

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