1-N-(4-methylphenylsulfonyl)amino-2-O-(4-methylphenylsulfonyl)oxycyclohexane

Base Information

Chemical Name:1-N-(4-methylphenylsulfonyl)amino-2-O-(4-methylphenylsulfonyl)oxycyclohexane
CAS No.:857003-99-7
Molecular Formula:C₂₀H₂₅NO₅S₂
Molecular Weight:423.554
Hs Code.:

Synonyms:1-N-(4-methylphenylsulfonyl)amino-2-O-(4-methylphenylsulfonyl)oxycyclohexane

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Chemical Property of 1-N-(4-methylphenylsulfonyl)amino-2-O-(4-methylphenylsulfonyl)oxycyclohexane

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Technology Process of 1-N-(4-methylphenylsulfonyl)amino-2-O-(4-methylphenylsulfonyl)oxycyclohexane

There total 2 articles about 1-N-(4-methylphenylsulfonyl)amino-2-O-(4-methylphenylsulfonyl)oxycyclohexane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 58107-40-7,69291-83-4
trans-2-(N-tosylamino)-1-cyclohexanol

: 98-59-9
p-toluenesulfonyl chloride

: 857003-99-7
1-N-(4-methylphenylsulfonyl)amino-2-O-(4-methylphenylsulfonyl)oxycyclohexane

Guidance literature:: With pyridine; In dichloromethane; 1.) 0 deg C, 20 min, 2.) 40 deg C, 24 h;
DOI:10.1016/S0040-4020(99)00214-8

Reference yield:

: 70-55-3
toluene-4-sulfonamide

: 857003-99-7
1-N-(4-methylphenylsulfonyl)amino-2-O-(4-methylphenylsulfonyl)oxycyclohexane

Guidance literature:: Multi-step reaction with 2 steps

1: 93 percent / K₂CO₃, TEBA / dioxane / 12 h / 90 °C

2: 82 percent / pyridine / CH₂Cl₂ / 1.) 0 deg C, 20 min, 2.) 40 deg C, 24 h

With pyridine; N-benzyl-N,N,N-triethylammonium chloride; potassium carbonate; In 1,4-dioxane; dichloromethane;
DOI:10.1016/S0040-4020(99)00214-8

Reference yield: 96.0%

: 857003-99-7
1-N-(4-methylphenylsulfonyl)amino-2-O-(4-methylphenylsulfonyl)oxycyclohexane

: 68820-12-2
cyclohexyl-N-tosyl aziridine

Guidance literature:: With potassium carbonate; In acetonitrile; at 45 ℃; for 0.666667h; other reagent, other temperature, other time;
DOI:10.1016/S0040-4020(99)00214-8