C₂₃H₂₃N₅O

Base Information

Chemical Name:C₂₃H₂₃N₅O
CAS No.:1398592-36-3
Molecular Formula:C₂₃H₂₃N₅O
Molecular Weight:385.469
Hs Code.:

C<sub>23</sub>H<sub>23</sub>N<sub>5</sub>O

Synonyms:C₂₃H₂₃N₅O

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Chemical Property of C₂₃H₂₃N₅O

Chemical Property:

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Technology Process of C₂₃H₂₃N₅O

There total 3 articles about C₂₃H₂₃N₅O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 1398592-35-2
C₂₃H₂₃BrN₂O

: 1398592-36-3
C₂₃H₂₃N₅O

Guidance literature:: With sodium azide; 18-crown-6 ether; tetra-(n-butyl)ammonium iodide; In N,N-dimethyl-formamide; at 55 ℃; for 12h;
DOI:10.1021/jo3016659

Reference yield:

: 72621-19-3
4-(4-bromobutoxy)benzaldehyde

: 1398592-36-3
C₂₃H₂₃N₅O

Guidance literature:: Multi-step reaction with 2 steps

1: potassium hexamethylsilazane / tetrahydrofuran; toluene / 3 h / 0 - 20 °C

2: sodium azide; 18-crown-6 ether; tetra-(n-butyl)ammonium iodide / N,N-dimethyl-formamide / 12 h / 55 °C

With sodium azide; 18-crown-6 ether; tetra-(n-butyl)ammonium iodide; potassium hexamethylsilazane; In tetrahydrofuran; N,N-dimethyl-formamide; toluene; 1: |Horner-Wadsworth-Emmons Olefination;
DOI:10.1021/jo3016659

Reference yield:

: 123-08-0,65581-83-1
4-hydroxy-benzaldehyde

: 1398592-36-3
C₂₃H₂₃N₅O

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate / acetonitrile / 12 h / Reflux

2: potassium hexamethylsilazane / tetrahydrofuran; toluene / 3 h / 0 - 20 °C

3: sodium azide; 18-crown-6 ether; tetra-(n-butyl)ammonium iodide / N,N-dimethyl-formamide / 12 h / 55 °C

With sodium azide; 18-crown-6 ether; tetra-(n-butyl)ammonium iodide; potassium hexamethylsilazane; potassium carbonate; In tetrahydrofuran; N,N-dimethyl-formamide; toluene; acetonitrile; 2: |Horner-Wadsworth-Emmons Olefination;
DOI:10.1021/jo3016659