diethyl 1,1'-(biphenyl-4,4'-diyl)bis(2-benzoyl-5-phenyl-1H-pyrrole-3-carboxylate)

Base Information

Chemical Name:diethyl 1,1'-(biphenyl-4,4'-diyl)bis(2-benzoyl-5-phenyl-1H-pyrrole-3-carboxylate)
CAS No.:1396396-45-4
Molecular Formula:C₅₂H₄₀N₂O₆
Molecular Weight:788.899
Hs Code.:

Synonyms:diethyl 1,1'-(biphenyl-4,4'-diyl)bis(2-benzoyl-5-phenyl-1H-pyrrole-3-carboxylate)

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Chemical Property of diethyl 1,1'-(biphenyl-4,4'-diyl)bis(2-benzoyl-5-phenyl-1H-pyrrole-3-carboxylate)

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Technology Process of diethyl 1,1'-(biphenyl-4,4'-diyl)bis(2-benzoyl-5-phenyl-1H-pyrrole-3-carboxylate)

There total 3 articles about diethyl 1,1'-(biphenyl-4,4'-diyl)bis(2-benzoyl-5-phenyl-1H-pyrrole-3-carboxylate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 1396396-19-2
ethyl 2-benzoyl-1-(4-iodophenyl)-5-phenyl-1H-pyrrole-3-carboxylate

: 1396396-45-4
diethyl 1,1'-(biphenyl-4,4'-diyl)bis(2-benzoyl-5-phenyl-1H-pyrrole-3-carboxylate)

Guidance literature:: With tetrabutylammomium bromide; palladium diacetate; sodium carbonate; In water; N,N-dimethyl-formamide; isopropyl alcohol; at 95 ℃; for 24h; Inert atmosphere;
DOI:10.1016/j.bmcl.2012.06.100

Reference yield:

: 70-11-1
α-bromoacetophenone

: 1396396-45-4
diethyl 1,1'-(biphenyl-4,4'-diyl)bis(2-benzoyl-5-phenyl-1H-pyrrole-3-carboxylate)

Guidance literature:: Multi-step reaction with 2 steps

1.1: N,N-dimethyl-formamide / 1 h / 20 °C

1.2: 10 h / 50 °C

2.1: tetrabutylammomium bromide; palladium diacetate; sodium carbonate / water; N,N-dimethyl-formamide; isopropyl alcohol / 24 h / 95 °C / Inert atmosphere

With tetrabutylammomium bromide; palladium diacetate; sodium carbonate; In water; N,N-dimethyl-formamide; isopropyl alcohol;
DOI:10.1016/j.bmcl.2012.06.100

Reference yield:

: 540-37-4
p-aminoiodobenzene

: 1396396-45-4
diethyl 1,1'-(biphenyl-4,4'-diyl)bis(2-benzoyl-5-phenyl-1H-pyrrole-3-carboxylate)

Guidance literature:: Multi-step reaction with 2 steps

1.1: N,N-dimethyl-formamide / 1 h / 20 °C

1.2: 10 h / 50 °C

2.1: tetrabutylammomium bromide; palladium diacetate; sodium carbonate / water; N,N-dimethyl-formamide; isopropyl alcohol / 24 h / 95 °C / Inert atmosphere

With tetrabutylammomium bromide; palladium diacetate; sodium carbonate; In water; N,N-dimethyl-formamide; isopropyl alcohol;
DOI:10.1016/j.bmcl.2012.06.100