phenyl-N-[(1-phenyl-1H-1,2,3-triazol-4-yl)methylene]methanamine

Base Information

Chemical Name:phenyl-N-[(1-phenyl-1H-1,2,3-triazol-4-yl)methylene]methanamine
CAS No.:133902-48-4
Molecular Formula:C₁₆H₁₄N₄
Molecular Weight:262.314
Hs Code.:
Mol file:133902-48-4.mol

Synonyms:Benzyl-[1-(1-phenyl-1H-[1,2,3]triazol-4-yl)-meth-(E)-ylidene]-amine

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Chemical Property of phenyl-N-[(1-phenyl-1H-1,2,3-triazol-4-yl)methylene]methanamine

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Technology Process of phenyl-N-[(1-phenyl-1H-1,2,3-triazol-4-yl)methylene]methanamine

There total 10 articles about phenyl-N-[(1-phenyl-1H-1,2,3-triazol-4-yl)methylene]methanamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 34296-51-0
1-phenyl-1,2,3-triazole-4-carbaldehyde

: 100-46-9
benzylamine

: 133902-48-4
Benzyl-[1-(1-phenyl-1H-[1,2,3]triazol-4-yl)-meth-(E)-ylidene]-amine

Guidance literature:: In methanol; for 24h; Ambient temperature;

Reference yield:

: 1516-60-5
4-nitrophenyl azide

: 133902-48-4
Benzyl-[1-(1-phenyl-1H-[1,2,3]triazol-4-yl)-meth-(E)-ylidene]-amine

Guidance literature:: Multi-step reaction with 6 steps

1: 71 percent / toluene / Heating

2: 36 percent / NaBH₄ / methanol / 1 h / Heating

3: 47 percent / MnO₂ / CH₂Cl₂ / Ambient temperature

4: 51 percent / ethanol / Ambient temperature

5: 2) HCOOH / 1) 80 deg C, DMSO, overnight, 2) H₂O, MeOH, reflux, 12 h

6: 84 percent / methanol / 24 h / Ambient temperature

With manganese(IV) oxide; sodium tetrahydroborate; formic acid; In methanol; ethanol; dichloromethane; toluene;

Reference yield:

: 103755-58-4
(1-phenyl-1H-1,2,3-triazole-4-yl)methanol

: 133902-48-4
Benzyl-[1-(1-phenyl-1H-[1,2,3]triazol-4-yl)-meth-(E)-ylidene]-amine

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / MnO₂ / CH₂Cl₂ / Ambient temperature

2: 84 percent / methanol / 24 h / Ambient temperature

With manganese(IV) oxide; In methanol; dichloromethane;