ethyl 6,7-dihydro-7,7-dimethyl-5-oxo-1-phenyl-1H,5H-pyrazolo[1,2-a]pyrazole-2-carboxylate

Base Information

Chemical Name:ethyl 6,7-dihydro-7,7-dimethyl-5-oxo-1-phenyl-1H,5H-pyrazolo[1,2-a]pyrazole-2-carboxylate
CAS No.:1152443-07-6
Molecular Formula:C₁₇H₂₀N₂O₃
Molecular Weight:300.357
Hs Code.:

Synonyms:ethyl 6,7-dihydro-7,7-dimethyl-5-oxo-1-phenyl-1H,5H-pyrazolo[1,2-a]pyrazole-2-carboxylate

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Chemical Property of ethyl 6,7-dihydro-7,7-dimethyl-5-oxo-1-phenyl-1H,5H-pyrazolo[1,2-a]pyrazole-2-carboxylate

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Technology Process of ethyl 6,7-dihydro-7,7-dimethyl-5-oxo-1-phenyl-1H,5H-pyrazolo[1,2-a]pyrazole-2-carboxylate

There total 8 articles about ethyl 6,7-dihydro-7,7-dimethyl-5-oxo-1-phenyl-1H,5H-pyrazolo[1,2-a]pyrazole-2-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 42953-83-3
1-benzylidene-5,5-dimethyl-3-oxopyrazolidin-1-ium-2-ide

: 623-47-2
propynoic acid ethyl ester

: 1152443-07-6
ethyl 6,7-dihydro-7,7-dimethyl-5-oxo-1-phenyl-1H,5H-pyrazolo[1,2-a]pyrazole-2-carboxylate

Guidance literature:: With copper(I)-USY zeolite; In toluene; at 60 ℃; for 4h;
DOI:10.1055/s-0029-1218733

Reference yield: 80.0%

: 59938-67-9
ethyl [²H]-propiolate

: 42953-83-3
1-benzylidene-5,5-dimethyl-3-oxopyrazolidin-1-ium-2-ide

: 1152443-07-6
ethyl 6,7-dihydro-7,7-dimethyl-5-oxo-1-phenyl-1H,5H-pyrazolo[1,2-a]pyrazole-2-carboxylate

: 1152443-60-1
C₁₇H₁₉⁽²⁾HN₂O₃

Guidance literature:: With copper(I)-exchanged deuterated zeolite; In toluene; at 60 ℃; for 4h; Reagent/catalyst; regioselective reaction; Mechanism; Inert atmosphere;
DOI:10.1002/chem.200802191

Reference yield:

: 4973-66-4
methyl thiotosylate

: 42953-83-3
1-benzylidene-5,5-dimethyl-3-oxopyrazolidin-1-ium-2-ide

: 623-47-2
propynoic acid ethyl ester

: 1152443-07-6
ethyl 6,7-dihydro-7,7-dimethyl-5-oxo-1-phenyl-1H,5H-pyrazolo[1,2-a]pyrazole-2-carboxylate

: ethyl 7,7-dimethyl-3-(methylthio)-5-oxo-1-phenyl-1,5,6,7-tetrahydropyrazolo[1,2-a]pyrazole-2-carboxylate

Guidance literature:: With copper(l) iodide; caesium carbonate; In 1,2-dichloro-ethane; at 45 ℃; for 12h; Reagent/catalyst; Inert atmosphere;
DOI:10.1002/adsc.201700387