di(tert-butyl) 2,2'-<<4-(4-aminobenzyl)-6-<4-<6-<amino>methyl>pyridin-2-yl>thiazol-2-yl>pyridin-2-yl>methylimino>bis(acetate)

Base Information

Chemical Name:di(tert-butyl) 2,2'-<<4-(4-aminobenzyl)-6-<4-<6-<amino>methyl>pyridin-2-yl>thiazol-2-yl>pyridin-2-yl>methylimino>bis(acetate)
CAS No.:150223-73-7
Molecular Formula:C₄₆H₆₂N₆O₈S
Molecular Weight:859.1
Hs Code.:

di(tert-butyl) 2,2'-<<4-(4-aminobenzyl)-6-<4-<6-<<bis<(tert-butoxy)carbonylmethyl>amino>methyl>pyridin-2-yl>thiazol-2-yl>pyridin-2-yl>methylimino>bis(acetate)

Synonyms:di(tert-butyl) 2,2'-<<4-(4-aminobenzyl)-6-<4-<6-<amino>methyl>pyridin-2-yl>thiazol-2-yl>pyridin-2-yl>methylimino>bis(acetate)

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Chemical Property of di(tert-butyl) 2,2'-<<4-(4-aminobenzyl)-6-<4-<6-<amino>methyl>pyridin-2-yl>thiazol-2-yl>pyridin-2-yl>methylimino>bis(acetate)

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Technology Process of di(tert-butyl) 2,2'-<<4-(4-aminobenzyl)-6-<4-<6-<amino>methyl>pyridin-2-yl>thiazol-2-yl>pyridin-2-yl>methylimino>bis(acetate)

There total 9 articles about di(tert-butyl) 2,2'-<<4-(4-aminobenzyl)-6-<4-<6-<amino>methyl>pyridin-2-yl>thiazol-2-yl>pyridin-2-yl>methylimino>bis(acetate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 27.0%

: 150223-71-5
di(tert-butyl) 2,2'-<<6-<4-<6-<amino>methyl>pyridin-2-yl>thiazol-2-yl>-4-(4-nitrobenzyl)pyridin-2-yl>methylimino>bis(acetate)

: 150223-73-7
di(tert-butyl) 2,2'-<<4-(4-aminobenzyl)-6-<4-<6-<amino>methyl>pyridin-2-yl>thiazol-2-yl>pyridin-2-yl>methylimino>bis(acetate)

Guidance literature:: With hydrogen; palladium on activated charcoal; In methanol; for 5h; under 5175.4 Torr;
DOI:10.1002/hlca.19960790129

Reference yield:

: 1083-48-3
4-Nitrobenzylpyridin

: 150223-73-7
di(tert-butyl) 2,2'-<<4-(4-aminobenzyl)-6-<4-<6-<amino>methyl>pyridin-2-yl>thiazol-2-yl>pyridin-2-yl>methylimino>bis(acetate)

Guidance literature:: Multi-step reaction with 9 steps

1: 83 percent / 3-chloroperbenzoic acid (50-55percent) / CH₂Cl₂ / 2 h

2: 53 percent / benzoyl chloride / CH₂Cl₂ / 0.5 h

3: 60 percent / NH₃ satd. in EtOH, H₂S / ethanol; CH₂Cl₂

4: 61 percent / ethanol / 3 h / Heating

5: 82 percent / 3-chloroperbenzoic acid (50-55percent) / CH₂Cl₂

6: 69 percent / benzoyl chloride / CH₂Cl₂

7: 1M BH₃*THF / tetrahydrofuran / 24 h

8: (i-Pr)2NEt / acetonitrile / 23 h / Heating

9: 27 percent / H₂ / 10percent Pd-C / methanol / 5 h / 5175.4 Torr

With borane-THF; hydrogen sulfide; ammonia; hydrogen; benzoyl chloride; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid; palladium on activated charcoal; In tetrahydrofuran; methanol; ethanol; dichloromethane; acetonitrile;
DOI:10.1002/hlca.19960790129

Reference yield:

: 26199-99-5
4-(4-nitrobenzyl)pyridine N-oxide

: 150223-73-7
di(tert-butyl) 2,2'-<<4-(4-aminobenzyl)-6-<4-<6-<amino>methyl>pyridin-2-yl>thiazol-2-yl>pyridin-2-yl>methylimino>bis(acetate)

Guidance literature:: Multi-step reaction with 8 steps

1: 53 percent / benzoyl chloride / CH₂Cl₂ / 0.5 h

2: 60 percent / NH₃ satd. in EtOH, H₂S / ethanol; CH₂Cl₂

3: 61 percent / ethanol / 3 h / Heating

4: 82 percent / 3-chloroperbenzoic acid (50-55percent) / CH₂Cl₂

5: 69 percent / benzoyl chloride / CH₂Cl₂

6: 1M BH₃*THF / tetrahydrofuran / 24 h

7: (i-Pr)2NEt / acetonitrile / 23 h / Heating

8: 27 percent / H₂ / 10percent Pd-C / methanol / 5 h / 5175.4 Torr

With borane-THF; hydrogen sulfide; ammonia; hydrogen; benzoyl chloride; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid; palladium on activated charcoal; In tetrahydrofuran; methanol; ethanol; dichloromethane; acetonitrile;
DOI:10.1002/hlca.19960790129