26199-99-5Relevant articles and documents
The M?CPbA?NH3(G) system: A safe and scalable alternative for the manufacture of (substituted) pyridine and quinoline N?oxides?
Palav, Amey,Misal, Balu,Ernolla, Anilkumar,Parab, Vinod,Waske, Prashant,Khandekar, Dileep,Chaudhary, Vinay,Chaturbhuj, Ganesh
supporting information, p. 244 - 251 (2019/03/17)
An improved, safe, and scalable isolation process for (substituted) pyridine and quinoline N-oxides in quantitative yields along with high purities using the m-CPBA?NH3(g) system is described. The safety was assessed by reaction calorimetry and differential scanning calorimetry studies for possible hazards during the conversion and isolation steps. Careful interpretation of the data substantiated the safety and scalability. The process flow is simplified to meet the industrial requirements of safety, cost-effectiveness, and utility minimization. The reaction was safely demonstrated at a 2.5 kg scale.
28. Novel thiazole-containing complexing agents and luminescence of their europium(III) and terbium(III) chelates
Mukkala, Veli-Matti,Liitti, Paeivi,Hemmilae, Ilkka,Takalo, Harri,Matachescu, Cristina,Kankare, Jouko
, p. 295 - 306 (2007/10/03)
The synthesis of novel thiazole-containing complexing agents and their luminescence properties with EuIII and TbIII ions are reported. One of these terpyridine analogues was also tested as an EuIII labelling reagent, and its luminescence properties as an antibody conjugate were studied.
Reactions of quinoline N-oxides and nitrobenzenes with methylquinoline and -pyridine derivatives in the presence of t-BuOK
Iwasaki, Genji,Saeki, Seitaro,Wada, Kazuko,Hamana, Masatomo
, p. 175 (2007/10/02)
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