2-<<<<(1,1-dimethylethyl)oxy>carbonyl>amino>methyl>-4-(1,1-dimethylethyl)-6-iodophenyl N,N-dimethylsulfamate

Base Information

Chemical Name:2-<<<<(1,1-dimethylethyl)oxy>carbonyl>amino>methyl>-4-(1,1-dimethylethyl)-6-iodophenyl N,N-dimethylsulfamate
CAS No.:68967-66-8
Molecular Formula:C₁₈H₂₉IN₂O₅S
Molecular Weight:512.409
Hs Code.:

Synonyms:2-<<<<(1,1-dimethylethyl)oxy>carbonyl>amino>methyl>-4-(1,1-dimethylethyl)-6-iodophenyl N,N-dimethylsulfamate

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Chemical Property of 2-<<<<(1,1-dimethylethyl)oxy>carbonyl>amino>methyl>-4-(1,1-dimethylethyl)-6-iodophenyl N,N-dimethylsulfamate

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Technology Process of 2-<<<<(1,1-dimethylethyl)oxy>carbonyl>amino>methyl>-4-(1,1-dimethylethyl)-6-iodophenyl N,N-dimethylsulfamate

There total 3 articles about 2-<<<<(1,1-dimethylethyl)oxy>carbonyl>amino>methyl>-4-(1,1-dimethylethyl)-6-iodophenyl N,N-dimethylsulfamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 68967-65-7
1,1-dimethylethyl N-<<5-(1,1-dimethylethyl)-2-hydroxy-3-iodophenyl>methyl>carbamate

: 13360-57-1
dimethylamino sulfonyl chloride

: 68967-66-8
2-<<<<(1,1-dimethylethyl)oxy>carbonyl>amino>methyl>-4-(1,1-dimethylethyl)-6-iodophenyl N,N-dimethylsulfamate

Guidance literature:: With triethylamine; In dichloromethane; at 20 - 25 ℃; for 72h;
DOI:10.1021/jm00348a024

Reference yield:

: 58456-91-0
2-aminomethyl-4-tert-butyl-6-iodophenol

: 68967-66-8
2-<<<<(1,1-dimethylethyl)oxy>carbonyl>amino>methyl>-4-(1,1-dimethylethyl)-6-iodophenyl N,N-dimethylsulfamate

Guidance literature:: Multi-step reaction with 2 steps

1: 79 percent / Et₃N / tetrahydrofuran; H₂O / 24 h / 60 - 65 °C

2: 63 percent / Et₃N / CH₂Cl₂ / 72 h / 20 - 25 °C

With triethylamine; In tetrahydrofuran; dichloromethane; water;
DOI:10.1021/jm00348a024

Reference yield:

: 16965-08-5
1,1-dimethylethyl 2,4,5-trichlorophenyl carbonate

: 68967-66-8
2-<<<<(1,1-dimethylethyl)oxy>carbonyl>amino>methyl>-4-(1,1-dimethylethyl)-6-iodophenyl N,N-dimethylsulfamate

Guidance literature:: Multi-step reaction with 2 steps

1: 79 percent / Et₃N / tetrahydrofuran; H₂O / 24 h / 60 - 65 °C

2: 63 percent / Et₃N / CH₂Cl₂ / 72 h / 20 - 25 °C

With triethylamine; In tetrahydrofuran; dichloromethane; water;
DOI:10.1021/jm00348a024