[Ni(Cl)(P(C₆H₃-3-SiMe₃-2-S)₃)]^-

Base Information

Chemical Name:[Ni(Cl)(P(C₆H₃-3-SiMe₃-2-S)₃)]^-
CAS No.:922725-12-0
Molecular Formula:C₂₇H₃₆ClNiPS₃Si₃*C₃₆H₃₀NP₂
Molecular Weight:1204.74
Hs Code.:

[Ni(Cl)(P(C<sub>6</sub>H<sub>3</sub>-3-SiMe<sub>3</sub>-2-S)<sub>3</sub>)]<sup>-</sup>

Synonyms:[Ni(Cl)(P(C₆H₃-3-SiMe₃-2-S)₃)]^-

Suppliers and Price of [Ni(Cl)(P(C₆H₃-3-SiMe₃-2-S)₃)]^-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of [Ni(Cl)(P(C₆H₃-3-SiMe₃-2-S)₃)]^-

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of [Ni(Cl)(P(C₆H₃-3-SiMe₃-2-S)₃)]^-

There total 4 articles about [Ni(Cl)(P(C₆H₃-3-SiMe₃-2-S)₃)]^- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 75-09-2
dichloromethane

: 922725-10-8
[bis(triphenylphosphoranylidene)ammonium][Ni(III)(SePh)(P(C₆H₃-3-SiMe₃-2-S)3)]

: 922725-12-0
(bis(triphenylphosphoranylidene))[NiCl(P(C₆H₃-3-SiMe₃-2-S)3]

Guidance literature:: In dichloromethane; (under N2, Schlenk); CH2Cl2 added to Ni-complex, stirred at ambient temp. for 48 h; hexane added, hexane diffused at room temp. for 1 wk; elem. anal.; Kinetics;
DOI:10.1021/ic061399g

Reference yield: 69.0%

: 956107-44-1
[bis(triphenylphosphoranylidene)ammonium][NiCl(P(o-C₆H₃-3-SiMe₃-2-S)2(o-C₆H₃-3-SiMe₃-2-SH))]

: 922725-12-0
[Ni(Cl)(P(C₆H₃-3-SiMe₃-2-S)₃)]^-

Guidance literature:: With 2,4,6-tri-tert-butyl phenoxyl radical; In tetrahydrofuran; at 23 ℃; Inert atmosphere; Schlenk technique;
DOI:10.1021/jacs.0c00712

Reference yield:

: 75-09-2
dichloromethane

: 922725-14-2
(bis(triphenylphosphoranylidene))[NiSC₂H₅(P(C₆H₃-3-SiMe₃-2-S)3]

: 922725-12-0
(bis(triphenylphosphoranylidene))[NiCl(P(C₆H₃-3-SiMe₃-2-S)3]

Guidance literature:: In dichloromethane; (under N2, Schlenk); CH2Cl2 added to Ni-complex, stirred at ambient temp. for 48 h; Kinetics;
DOI:10.1021/ic061399g