4-methoxy-thiobenzoic acid o-toluidide

Base Information

• Chemical Name: 4-methoxy-thiobenzoic acid o-toluidide
• CAS No.: 156085-86-8
• Molecular Formula: C₁₅H₁₅NOS
• Molecular Weight: 257.356
• Mol file: 156085-86-8.mol

Synonyms:4-methoxy-thiobenzoic acid o-toluidide

Chemical Property of 4-methoxy-thiobenzoic acid o-toluidide

Chemical Property:

Purity/Quality:

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Technology Process of 4-methoxy-thiobenzoic acid o-toluidide

There total 2 articles about 4-methoxy-thiobenzoic acid o-toluidide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

4-methoxy-N-(2-methylphenyl)benzamide (7464-54-2) → 4-methoxy-thiobenzoic acid o-toluidide (156085-86-8)

Guidance literature:

With Lawessons reagent; In chlorobenzene; for 3h; Heating;

DOI:10.1021/jm00037a020

Reference yield:

methoxybenzene (100-66-3) + 2-tolyl isothiocyanate (614-69-7) → 4-methoxy-thiobenzoic acid o-toluidide (156085-86-8)

Guidance literature:

With carbon disulfide; aluminium trichloride;

Reference yield: 90.0%

4-methoxy-thiobenzoic acid o-toluidide (156085-86-8) → 2-(4-methoxyphenyl)-4-methylbenzo[d]thiazole

Guidance literature:

With sodium hydroxide; potassium hexacyanoferrate(III); for 0.5h; Heating;

DOI:10.1021/jm00037a020

upstream raw materials:

methoxybenzene

2-tolyl isothiocyanate

4-methoxy-N-(2-methylphenyl)benzamide

Refernces