4-oxido-4-(2-{[1-oxo-3-phenyl-2-(pyridin-3-yl)-1H-inden-6-yl]oxy}ethyl)morpholin-4-ium

Base Information

Chemical Name:4-oxido-4-(2-{[1-oxo-3-phenyl-2-(pyridin-3-yl)-1H-inden-6-yl]oxy}ethyl)morpholin-4-ium
CAS No.:1274878-97-5
Molecular Formula:C₂₆H₂₄N₂O₄
Molecular Weight:428.488
Hs Code.:

Synonyms:4-oxido-4-(2-{[1-oxo-3-phenyl-2-(pyridin-3-yl)-1H-inden-6-yl]oxy}ethyl)morpholin-4-ium

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Chemical Property of 4-oxido-4-(2-{[1-oxo-3-phenyl-2-(pyridin-3-yl)-1H-inden-6-yl]oxy}ethyl)morpholin-4-ium

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Technology Process of 4-oxido-4-(2-{[1-oxo-3-phenyl-2-(pyridin-3-yl)-1H-inden-6-yl]oxy}ethyl)morpholin-4-ium

There total 9 articles about 4-oxido-4-(2-{[1-oxo-3-phenyl-2-(pyridin-3-yl)-1H-inden-6-yl]oxy}ethyl)morpholin-4-ium which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 13.0%

: 1274877-35-8
6-(2-morpholinoethoxy)-3-phenyl-2-(pyridin-3-yl)-1H-inden-1-one

: 1274878-97-5
4-oxido-4-(2-{[1-oxo-3-phenyl-2-(pyridin-3-yl)-1H-inden-6-yl]oxy}ethyl)morpholin-4-ium

: 1274878-98-6
4-oxido-4-(2-{[2-(1-oxidopyridin-1-ium-3-yl)-1-oxo-3-phenyl-1H-inden-6-yl]oxy}ethyl)morpholin-4-ium

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 10 - 20 ℃; for 2h;

Reference yield:

: 1274877-34-7
6-(2-morpholinoethoxy)-2-bromo-3-phenyl-1H-inden-1-one

: 1274878-97-5
4-oxido-4-(2-{[1-oxo-3-phenyl-2-(pyridin-3-yl)-1H-inden-6-yl]oxy}ethyl)morpholin-4-ium

: 1274878-98-6
4-oxido-4-(2-{[2-(1-oxidopyridin-1-ium-3-yl)-1-oxo-3-phenyl-1H-inden-6-yl]oxy}ethyl)morpholin-4-ium

Guidance literature:: Multi-step reaction with 2 steps

1: sodium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,4-dioxane; water / 0.33 h / 150 °C / Microwave Irradiation

2: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 2 h / 10 - 20 °C

With sodium carbonate; 3-chloro-benzenecarboperoxoic acid; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In 1,4-dioxane; dichloromethane; water; 1: Suzuki Coupling;

Reference yield:

: 100-52-7
benzaldehyde

: 1274878-97-5
4-oxido-4-(2-{[1-oxo-3-phenyl-2-(pyridin-3-yl)-1H-inden-6-yl]oxy}ethyl)morpholin-4-ium

: 1274878-98-6
4-oxido-4-(2-{[2-(1-oxidopyridin-1-ium-3-yl)-1-oxo-3-phenyl-1H-inden-6-yl]oxy}ethyl)morpholin-4-ium

Guidance literature:: Multi-step reaction with 8 steps

1: sodium hydroxide / ethanol; water / 27.5 h / 10 - 20 °C

2: trifluoroacetic acid / 24 h / 80 °C

3: pyridine / dichloromethane / 8 h / 0 - 20 °C

4: 2,2'-azobis(isobutyronitrile); N-Bromosuccinimide / tetrachloromethane / 2.5 h / Reflux; Irradiation

5: potassium carbonate; methanol / 2 h / 20 °C

6: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 2.5 h / 0 - 20 °C

7: sodium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,4-dioxane; water / 0.33 h / 150 °C / Microwave Irradiation

8: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 2 h / 10 - 20 °C

With methanol; N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); di-isopropyl azodicarboxylate; sodium carbonate; potassium carbonate; 3-chloro-benzenecarboperoxoic acid; triphenylphosphine; trifluoroacetic acid; sodium hydroxide; pyridine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; 1,4-dioxane; tetrachloromethane; ethanol; dichloromethane; water; 6: Mitsunobu reaction / 7: Suzuki Coupling;