C₃₄H₃₈FN₃O₈

Base Information

Chemical Name:C₃₄H₃₈FN₃O₈
CAS No.:1381849-07-5
Molecular Formula:C₃₄H₃₈FN₃O₈
Molecular Weight:635.689
Hs Code.:

C<sub>34</sub>H<sub>38</sub>FN<sub>3</sub>O<sub>8</sub>

Synonyms:C₃₄H₃₈FN₃O₈

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Chemical Property of C₃₄H₃₈FN₃O₈

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Technology Process of C₃₄H₃₈FN₃O₈

There total 4 articles about C₃₄H₃₈FN₃O₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 1381849-06-4
C₄₈H₅₀FN₃O₈

: 1381849-07-5
C₃₄H₃₈FN₃O₈

Guidance literature:: With palladium 10% on activated carbon; hydrogen; In tetrahydrofuran; water; at 20 ℃; for 3h;
DOI:10.1016/j.bmc.2012.04.034

Reference yield:

: 1381849-03-1
benzyl 2-(4-hydroxy-2-methylbutan-2-yl)-3,5-dimethylphenyl succinate

: 1381849-07-5
C₃₄H₃₈FN₃O₈

Guidance literature:: Multi-step reaction with 4 steps

1.1: pyridinium chlorochromate / dichloromethane / 3 h / 20 °C / Inert atmosphere

2.1: sodium dihydrogenphosphate; sodium chlorite; water; dihydrogen peroxide / acetonitrile / 0 - 20 °C / Inert atmosphere

2.2: pH 2 / Inert atmosphere

3.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 0.08 h / 0 °C / Inert atmosphere

3.2: 0 - 20 °C / Inert atmosphere

4.1: palladium 10% on activated carbon; hydrogen / tetrahydrofuran; water / 3 h / 20 °C

With sodium chlorite; sodium dihydrogenphosphate; palladium 10% on activated carbon; water; hydrogen; dihydrogen peroxide; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; pyridinium chlorochromate; In tetrahydrofuran; dichloromethane; water; acetonitrile;
DOI:10.1016/j.bmc.2012.04.034

Reference yield:

: 134098-64-9
2‐{3‐[(O‐tert‐butyldimethylsilyl)hydroxy]‐1,1‐dimethylpropyl}‐3,5‐dimethylphenol

: 1381849-07-5
C₃₄H₃₈FN₃O₈

Guidance literature:: Multi-step reaction with 6 steps

1.1: dicyclohexyl-carbodiimide / dichloromethane / 0.17 h / 0 °C / Inert atmosphere

1.2: 0 - 23 °C / Inert atmosphere

2.1: water; acetic acid / tetrahydrofuran / 3 h / 20 °C / Inert atmosphere

3.1: pyridinium chlorochromate / dichloromethane / 3 h / 20 °C / Inert atmosphere

4.1: sodium dihydrogenphosphate; sodium chlorite; water; dihydrogen peroxide / acetonitrile / 0 - 20 °C / Inert atmosphere

4.2: pH 2 / Inert atmosphere

5.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 0.08 h / 0 °C / Inert atmosphere

5.2: 0 - 20 °C / Inert atmosphere

6.1: palladium 10% on activated carbon; hydrogen / tetrahydrofuran; water / 3 h / 20 °C

With sodium chlorite; sodium dihydrogenphosphate; palladium 10% on activated carbon; water; hydrogen; dihydrogen peroxide; benzotriazol-1-ol; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dicyclohexyl-carbodiimide; pyridinium chlorochromate; In tetrahydrofuran; dichloromethane; water; acetonitrile;
DOI:10.1016/j.bmc.2012.04.034