N-(2-aminoethyl)-4-[5-(4-dimethylaminophenyl)oxazol-2-yl]benzenesulfonamide

Base Information

Chemical Name:N-(2-aminoethyl)-4-[5-(4-dimethylaminophenyl)oxazol-2-yl]benzenesulfonamide
CAS No.:203250-31-1
Molecular Formula:C₁₉H₂₂N₄O₃S
Molecular Weight:386.475
Hs Code.:

Synonyms:N-(2-aminoethyl)-4-[5-(4-dimethylaminophenyl)oxazol-2-yl]benzenesulfonamide

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Chemical Property of N-(2-aminoethyl)-4-[5-(4-dimethylaminophenyl)oxazol-2-yl]benzenesulfonamide

Chemical Property:

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Technology Process of N-(2-aminoethyl)-4-[5-(4-dimethylaminophenyl)oxazol-2-yl]benzenesulfonamide

There total 5 articles about N-(2-aminoethyl)-4-[5-(4-dimethylaminophenyl)oxazol-2-yl]benzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 102742-20-1
2-amino-4'-dimethylaminoacetophenone hydrochloride

: 203250-31-1
N-(2-aminoethyl)-4-[5-(4-dimethylaminophenyl)oxazol-2-yl]benzenesulfonamide

Guidance literature:: Multi-step reaction with 5 steps

1: 95 percent / pyridine / CH₂Cl₂ / 12 h / Ambient temperature

2: 92 percent / conc. H₂SO₄ / 24 h

3: 86 percent / 10percent aq. NaOH / 2 h / Heating

4: 81 percent / POCl₃ / 1 h / Heating

5: 46 percent / CH₂Cl₂; dimethylformamide / 12 h / Ambient temperature

With pyridine; sodium hydroxide; sulfuric acid; trichlorophosphate; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1111/j.1751-1097.1997.tb03168.x

Reference yield:

: 138219-56-4
4-(5-dimethylaminophenyl-2-oxazolyl)benzenesulfonyl fluoride

: 203250-31-1
N-(2-aminoethyl)-4-[5-(4-dimethylaminophenyl)oxazol-2-yl]benzenesulfonamide

Guidance literature:: Multi-step reaction with 3 steps

1: 86 percent / 10percent aq. NaOH / 2 h / Heating

2: 81 percent / POCl₃ / 1 h / Heating

3: 46 percent / CH₂Cl₂; dimethylformamide / 12 h / Ambient temperature

With sodium hydroxide; trichlorophosphate; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1111/j.1751-1097.1997.tb03168.x

Reference yield:

: dapoxyl sodium sulfonate

: 203250-31-1
N-(2-aminoethyl)-4-[5-(4-dimethylaminophenyl)oxazol-2-yl]benzenesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: 81 percent / POCl₃ / 1 h / Heating

2: 46 percent / CH₂Cl₂; dimethylformamide / 12 h / Ambient temperature

With trichlorophosphate; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1111/j.1751-1097.1997.tb03168.x