methyl 2-<4'-methoxy-2'-(methoxymethoxy)phenoxy>-3-(3'',4''-methylenedioxyphenyl)-3-oxopropionate

Base Information

Chemical Name:methyl 2-<4'-methoxy-2'-(methoxymethoxy)phenoxy>-3-(3'',4''-methylenedioxyphenyl)-3-oxopropionate
CAS No.:124872-82-8
Molecular Formula:C₂₀H₂₀O₉
Molecular Weight:404.373
Hs Code.:

Synonyms:methyl 2-<4'-methoxy-2'-(methoxymethoxy)phenoxy>-3-(3'',4''-methylenedioxyphenyl)-3-oxopropionate

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Chemical Property of methyl 2-<4'-methoxy-2'-(methoxymethoxy)phenoxy>-3-(3'',4''-methylenedioxyphenyl)-3-oxopropionate

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Technology Process of methyl 2-<4'-methoxy-2'-(methoxymethoxy)phenoxy>-3-(3'',4''-methylenedioxyphenyl)-3-oxopropionate

There total 6 articles about methyl 2-<4'-methoxy-2'-(methoxymethoxy)phenoxy>-3-(3'',4''-methylenedioxyphenyl)-3-oxopropionate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 123913-92-8
4-methoxy-2-(methoxymethoxy)phenol

: 124872-81-7
methyl 2-bromo-2-(3',4'-methylenedioxybenzoyl)acetate

: 124872-82-8
methyl 2-<4'-methoxy-2'-(methoxymethoxy)phenoxy>-3-(3'',4''-methylenedioxyphenyl)-3-oxopropionate

Guidance literature:: With dibenzo-18-crown-6; potassium tert-butylate; In acetonitrile;

Reference yield:

: 673-22-3
2-Hydroxy-4-methoxybenzaldehyde

: 124872-82-8
methyl 2-<4'-methoxy-2'-(methoxymethoxy)phenoxy>-3-(3'',4''-methylenedioxyphenyl)-3-oxopropionate

Guidance literature:: Multi-step reaction with 4 steps

1: 79 percent / KOH / dibenzo-18-crown-6 / acetonitrile / 6 h / Ambient temperature

2: m-chloroperbenzoic acid, KF / CH₂Cl₂ / 42 h / Ambient temperature

3: aq. NaOH / 0.5 h / Ambient temperature

4: 94 percent / tert-BuOK / dibenzo-18-crown-6 / acetonitrile / 14 h / Ambient temperature

With potassium fluoride; potassium hydroxide; potassium tert-butylate; 3-chloro-benzenecarboperoxoic acid; dibenzo-18-crown-6; In sodium hydroxide; dichloromethane; acetonitrile;

Reference yield:

: 124555-63-1
4-methoxy-2-methoxymethoxy benzaldehyde

: 124872-82-8
methyl 2-<4'-methoxy-2'-(methoxymethoxy)phenoxy>-3-(3'',4''-methylenedioxyphenyl)-3-oxopropionate

Guidance literature:: Multi-step reaction with 3 steps

1: m-chloroperbenzoic acid, KF / CH₂Cl₂ / 42 h / Ambient temperature

2: aq. NaOH / 0.5 h / Ambient temperature

3: 94 percent / tert-BuOK / dibenzo-18-crown-6 / acetonitrile / 14 h / Ambient temperature

With potassium fluoride; potassium tert-butylate; 3-chloro-benzenecarboperoxoic acid; dibenzo-18-crown-6; In sodium hydroxide; dichloromethane; acetonitrile;