(E)-2-(4-chlorophenyl)-N-(5,6,7,8-tetrahydronaphthalen-1-yl)acetimidoyl chloride

Base Information

Chemical Name:(E)-2-(4-chlorophenyl)-N-(5,6,7,8-tetrahydronaphthalen-1-yl)acetimidoyl chloride
CAS No.:924633-61-4
Molecular Formula:C₁₈H₁₇Cl₂N
Molecular Weight:318.246
Hs Code.:

Synonyms:(E)-2-(4-chlorophenyl)-N-(5,6,7,8-tetrahydronaphthalen-1-yl)acetimidoyl chloride

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-2-(4-chlorophenyl)-N-(5,6,7,8-tetrahydronaphthalen-1-yl)acetimidoyl chloride

Chemical Property:

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Technology Process of (E)-2-(4-chlorophenyl)-N-(5,6,7,8-tetrahydronaphthalen-1-yl)acetimidoyl chloride

There total 3 articles about (E)-2-(4-chlorophenyl)-N-(5,6,7,8-tetrahydronaphthalen-1-yl)acetimidoyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 924633-60-3
2-(4-chlorophenyl)-N-(5,6,7,8-tetrahydronaphthalen-1-yl)acetamide

: 924633-61-4
(E)-2-(4-chlorophenyl)-N-(5,6,7,8-tetrahydronaphthalen-1-yl)acetimidoyl chloride

Guidance literature:: With phosphorus pentachloride; at 65 ℃; for 4h;
DOI:10.1021/jm060631p

Reference yield:

: 1878-66-6
4-chlorophenylacetic Acid

: 924633-61-4
(E)-2-(4-chlorophenyl)-N-(5,6,7,8-tetrahydronaphthalen-1-yl)acetimidoyl chloride

Guidance literature:: Multi-step reaction with 3 steps

1: oxalyl chloride; DMF / tetrahydrofuran / 1 h

2: 90 percent / i-Pr₂NEt / CH₂Cl₂ / 20 °C

3: PCl₅ / 4 h / 65 °C

With oxalyl dichloride; phosphorus pentachloride; N-ethyl-N,N-diisopropylamine; N,N-dimethyl-formamide; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jm060631p

Reference yield:

: 25026-34-0
4-chlorophenacetyl chloride

: 924633-61-4
(E)-2-(4-chlorophenyl)-N-(5,6,7,8-tetrahydronaphthalen-1-yl)acetimidoyl chloride

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / i-Pr₂NEt / CH₂Cl₂ / 20 °C

2: PCl₅ / 4 h / 65 °C

With phosphorus pentachloride; N-ethyl-N,N-diisopropylamine; In dichloromethane;
DOI:10.1021/jm060631p