2-(6-dimethylaminohexylthio)-5-(2-chlorophenyl)-7-chloro-3H-1,4-benzodiazepine

Base Information

Chemical Name:2-(6-dimethylaminohexylthio)-5-(2-chlorophenyl)-7-chloro-3H-1,4-benzodiazepine
CAS No.:67974-48-5
Molecular Formula:C₂₃H₂₇Cl₂N₃S
Molecular Weight:448.459
Hs Code.:

Synonyms:2-(6-dimethylaminohexylthio)-5-(2-chlorophenyl)-7-chloro-3H-1,4-benzodiazepine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-(6-dimethylaminohexylthio)-5-(2-chlorophenyl)-7-chloro-3H-1,4-benzodiazepine

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Technology Process of 2-(6-dimethylaminohexylthio)-5-(2-chlorophenyl)-7-chloro-3H-1,4-benzodiazepine

There total 2 articles about 2-(6-dimethylaminohexylthio)-5-(2-chlorophenyl)-7-chloro-3H-1,4-benzodiazepine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.7%

: 68402-57-3
6-(N,N-dimethylamino)-1-hexanethiol

: 2894-67-9
delorazepam

: 67974-48-5
2-(6-dimethylaminohexylthio)-5-(2-chlorophenyl)-7-chloro-3H-1,4-benzodiazepine

Guidance literature:: With titanium tetrachloride; In toluene; for 1.5h; Heating;
DOI:10.1248/cpb.30.1473

Reference yield:

: 6-(N,N-dimethyl)amino-1-chlorohexane hydrochloride

: 2894-71-5,49853-64-7
7-chloro-1,3-dihydro-5-(o-chlorophenyl)-2H-1,4-benzodiazepine-2-thione

: 67974-48-5
2-(6-dimethylaminohexylthio)-5-(2-chlorophenyl)-7-chloro-3H-1,4-benzodiazepine

Guidance literature:: With potassium hydroxide; In tetrahydrofuran; water; for 1.5h; Yield given; Ambient temperature;
DOI:10.1248/cpb.30.1141