(η3-allyl)(2-(5-phenyl-1H-pyrazol-3-yl)pyridine)palladium(II) tetrafluoroborate

Base Information

Chemical Name:(η3-allyl)(2-(5-phenyl-1H-pyrazol-3-yl)pyridine)palladium(II) tetrafluoroborate
CAS No.:944162-92-9
Molecular Formula:BF₄*C₁₇H₁₆N₃Pd
Molecular Weight:455.559
Hs Code.:

Synonyms:(η3-allyl)(2-(5-phenyl-1H-pyrazol-3-yl)pyridine)palladium(II) tetrafluoroborate

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Chemical Property of (η3-allyl)(2-(5-phenyl-1H-pyrazol-3-yl)pyridine)palladium(II) tetrafluoroborate

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Technology Process of (η3-allyl)(2-(5-phenyl-1H-pyrazol-3-yl)pyridine)palladium(II) tetrafluoroborate

There total 1 articles about (η3-allyl)(2-(5-phenyl-1H-pyrazol-3-yl)pyridine)palladium(II) tetrafluoroborate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 14104-20-2
silver tetrafluoroborate

: bis(η3-allyl-μ-chloropalladium(II))

: 15395-62-7
2-(5-phenyl-1H-pyrazol-3-yl)-pyridine

: 944162-92-9
(η3-allyl)(2-(5-phenyl-1H-pyrazol-3-yl)pyridine)palladium(II) tetrafluoroborate

Guidance literature:: In dichloromethane; under N2, protected from light; ligand added to mixt. of AgBF4 and Pd complex in dry CH2Cl2 at 0°C; stirred at room temp. for 1.5 h; MeOH added; filtered through Celite; filtrate stirred for 1 h; most of solvent removed under vac.; Et2O added dropwise; filtered; solid rinsed with Et2O; dried under vac.; elem. anal.;
DOI:10.1021/om070093u

Reference yield: 60.0%

: 944162-92-9
(η3-allyl)(2-(5-phenyl-1H-pyrazol-3-yl)pyridine)palladium(II) tetrafluoroborate

: 944162-99-6
(η3-allyl)(2-(5-phenyl-1H-pyrazol-3-yl)pyridine(-1H))palladium(II)

Guidance literature:: With sodium methoxide; In methanol; dichloromethane; byproducts: NaBF4, MeOH; Sonication; under N2; CH2Cl2 and MeOH added to mixt. of Pd complex and NaOMe at roomtemp.; stirred with sonication for 5 min; solvent evapd.; rinsed with Et2O; dried under vac.; elem. anal.;
DOI:10.1021/om070093u