ethyl 2,2-difluoro-3-{[(methylthio)carbonothioyl]oxy}-3-phenyl propanoate

Base Information

Chemical Name:ethyl 2,2-difluoro-3-{[(methylthio)carbonothioyl]oxy}-3-phenyl propanoate
CAS No.:915133-84-5
Molecular Formula:C₁₃H₁₄F₂O₃S₂
Molecular Weight:320.381
Hs Code.:

Synonyms:ethyl 2,2-difluoro-3-{[(methylthio)carbonothioyl]oxy}-3-phenyl propanoate

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Chemical Property of ethyl 2,2-difluoro-3-{[(methylthio)carbonothioyl]oxy}-3-phenyl propanoate

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Technology Process of ethyl 2,2-difluoro-3-{[(methylthio)carbonothioyl]oxy}-3-phenyl propanoate

There total 1 articles about ethyl 2,2-difluoro-3-{[(methylthio)carbonothioyl]oxy}-3-phenyl propanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 92207-60-8
ethyl 2,2-difluoro-3-hydroxy-3-phenylpropanoate

: 74-88-4
methyl iodide

: 915133-84-5
ethyl 2,2-difluoro-3-{[(methylthio)carbonothioyl]oxy}-3-phenyl propanoate

Guidance literature:: carbon disulfide; ethyl 2,2-difluoro-3-hydroxy-3-phenylpropanoate; With 1,8-diazabicyclo[5.4.0]undec-7-ene; In N,N-dimethyl-formamide; at 20 ℃; for 1.5h;

methyl iodide; In N,N-dimethyl-formamide; at 20 ℃; for 1.5h;

Reference yield: 42.0%

: 915133-84-5
ethyl 2,2-difluoro-3-{[(methylthio)carbonothioyl]oxy}-3-phenyl propanoate

: 134806-69-2
ethyl 2,2-difluoro-3-phenylpropionate

Guidance literature:: With di-tert-butyl peroxide; Diphenylphosphine oxide; In 1,4-dioxane; at 110 ℃; for 48h;

Reference yield:

: 915133-84-5
ethyl 2,2-difluoro-3-{[(methylthio)carbonothioyl]oxy}-3-phenyl propanoate

: 915133-85-6
β,β-difluorobenzenepropanol

Guidance literature:: Multi-step reaction with 2 steps

1: di-tert-butyl peroxide; Diphenylphosphine oxide / 1,4-dioxane / 48 h / 110 °C

2: sodium tetrahydroborate / methanol / 2.33 h / 5 - 20 °C

With sodium tetrahydroborate; di-tert-butyl peroxide; Diphenylphosphine oxide; In 1,4-dioxane; methanol;