5α-androst[3,2-b][17,16-b][bis-{4'-(p-chlorophenyl)-6'-phenyl}]pyridine

Base Information

Chemical Name:5α-androst[3,2-b][17,16-b][bis-{4'-(p-chlorophenyl)-6'-phenyl}]pyridine
CAS No.:1428483-80-0
Molecular Formula:C₄₉H₄₄Cl₂N₂
Molecular Weight:731.808
Hs Code.:

Synonyms:5α-androst[3,2-b][17,16-b][bis-{4'-(p-chlorophenyl)-6'-phenyl}]pyridine

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Chemical Property of 5α-androst[3,2-b][17,16-b][bis-{4'-(p-chlorophenyl)-6'-phenyl}]pyridine

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Technology Process of 5α-androst[3,2-b][17,16-b][bis-{4'-(p-chlorophenyl)-6'-phenyl}]pyridine

There total 2 articles about 5α-androst[3,2-b][17,16-b][bis-{4'-(p-chlorophenyl)-6'-phenyl}]pyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 1428586-85-9
2,16-bis[1'-(p-chlorophenyl)-3'-phenyl-propyl-3'-one]-5α-antrost-3,17-dione

: 1428483-80-0
5α-androst[3,2-b][17,16-b][bis-{4'-(p-chlorophenyl)-6'-phenyl}]pyridine

Guidance literature:: With boron trifluoride diethyl etherate; urea; at 130 ℃; for 0.1h; under 15751.6 Torr; Microwave irradiation;
DOI:10.1016/j.steroids.2013.01.006

Reference yield:

: 846-46-8
androstanedione

: 104-88-1
4-chlorobenzaldehyde

: 98-86-2
acetophenone

: 1428483-80-0
5α-androst[3,2-b][17,16-b][bis-{4'-(p-chlorophenyl)-6'-phenyl}]pyridine

Guidance literature:: Multi-step reaction with 2 steps

1: potassium hydroxide / toluene / 6 h / 20 °C

2: urea; boron trifluoride diethyl etherate / 0.1 h / 130 °C / 15751.6 Torr / Microwave irradiation

With boron trifluoride diethyl etherate; urea; potassium hydroxide; In toluene;
DOI:10.1016/j.steroids.2013.01.006