p-methoxyphenyl 3,4,7-tri-O-benzyl-1-deoxy-1-ethoxysulfonyl-α-D-gluco-hept-2-ulopyranosyl-(2->4)-2,3,6-tri-O-benzyl-β-D-glucopyranoside

Base Information

Chemical Name:p-methoxyphenyl 3,4,7-tri-O-benzyl-1-deoxy-1-ethoxysulfonyl-α-D-gluco-hept-2-ulopyranosyl-(2->4)-2,3,6-tri-O-benzyl-β-D-glucopyranoside
CAS No.:1381871-21-1
Molecular Formula:C₆₄H₇₀O₁₅S
Molecular Weight:1111.32
Hs Code.:

Synonyms:p-methoxyphenyl 3,4,7-tri-O-benzyl-1-deoxy-1-ethoxysulfonyl-α-D-gluco-hept-2-ulopyranosyl-(2->4)-2,3,6-tri-O-benzyl-β-D-glucopyranoside

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Chemical Property of p-methoxyphenyl 3,4,7-tri-O-benzyl-1-deoxy-1-ethoxysulfonyl-α-D-gluco-hept-2-ulopyranosyl-(2->4)-2,3,6-tri-O-benzyl-β-D-glucopyranoside

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Technology Process of p-methoxyphenyl 3,4,7-tri-O-benzyl-1-deoxy-1-ethoxysulfonyl-α-D-gluco-hept-2-ulopyranosyl-(2->4)-2,3,6-tri-O-benzyl-β-D-glucopyranoside

There total 1 articles about p-methoxyphenyl 3,4,7-tri-O-benzyl-1-deoxy-1-ethoxysulfonyl-α-D-gluco-hept-2-ulopyranosyl-(2->4)-2,3,6-tri-O-benzyl-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 1381871-19-7
p-methoxyphenyl 3,4,7-tri-O-benzyl-5-O-((2-naphthyl)methyl)-1-deoxy-1-ethoxysulfonyl-α-D-gluco-hept-2-ulopyranosyl-(2->4)-2,3,6-tri-O-benzyl-β-D-glucopyranoside

: 1381871-21-1
p-methoxyphenyl 3,4,7-tri-O-benzyl-1-deoxy-1-ethoxysulfonyl-α-D-gluco-hept-2-ulopyranosyl-(2->4)-2,3,6-tri-O-benzyl-β-D-glucopyranoside

Guidance literature:: With water; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In dichloromethane; at 20 ℃; for 0.416667h; chemoselective reaction; Inert atmosphere;
DOI:10.1016/j.tet.2012.04.067

Reference yield: 62.0%

: 1381871-21-1
p-methoxyphenyl 3,4,7-tri-O-benzyl-1-deoxy-1-ethoxysulfonyl-α-D-gluco-hept-2-ulopyranosyl-(2->4)-2,3,6-tri-O-benzyl-β-D-glucopyranoside

: 1381871-32-4
p-methoxyphenyl 4-O-(1-deoxy-1-(sodium sulfonato)-α-D-gluco-hept-2-ulopyranosyl)-β-D-glucopyranoside

Guidance literature:: p-methoxyphenyl 3,4,7-tri-O-benzyl-1-deoxy-1-ethoxysulfonyl-α-D-gluco-hept-2-ulopyranosyl-(2->4)-2,3,6-tri-O-benzyl-β-D-glucopyranoside; With sodium iodide; In acetone; for 48h; Inert atmosphere;

With palladium 10% on activated carbon; hydrogen; In ethanol; water; ethyl acetate; under 15001.5 Torr; Autoclave;
DOI:10.1016/j.tet.2012.04.067

Reference yield:

: 1381871-17-5
3,4,7-tri-O-benzyl-5-O-((2-naphthyl)methyl)-1-deoxy-1-ethoxysulfonyl-α-D-gluco-hept-2-ulopyranosyl chloride

: 1381871-21-1
p-methoxyphenyl 3,4,7-tri-O-benzyl-1-deoxy-1-ethoxysulfonyl-α-D-gluco-hept-2-ulopyranosyl-(2->4)-2,3,6-tri-O-benzyl-β-D-glucopyranoside

: 1381871-20-0
2,6-anhydro-3,4,7-tri-O-benzyl-5-O-((2-naphthyl)methyl)-1-deoxy-1-ethoxysulfonyl-D-gluco-hept-1-enitol

: 1381871-22-2
p-methoxyphenyl 3,4,7-tri-O-benzyl-5-O-((2-naphthyl)methyl)-1-deoxy-1-ethoxysulfonyl-α-D-gluco-hept-2-ulopyranosyl-(2->5)-3,4,7-tri-O-benzyl-1-deoxy-1-ethoxysulfonyl-α-D-gluco-hept-2-ulopyranosyl-(2->4)-2,3,6-tri-O-benzyl-β-D-glucopyranoside

Guidance literature:: With silver trifluoromethanesulfonate; In dichloromethane; toluene; at 0 ℃; for 120h; Inert atmosphere; Molecular sieve;
DOI:10.1016/j.tet.2012.04.067