2,6-anhydro-3,4,7-tri-O-benzyl-5-O-((2-naphthyl)methyl)-1-deoxy-1-ethoxysulfonyl-D-gluco-hept-1-enitol

Base Information

Chemical Name:2,6-anhydro-3,4,7-tri-O-benzyl-5-O-((2-naphthyl)methyl)-1-deoxy-1-ethoxysulfonyl-D-gluco-hept-1-enitol
CAS No.:1381871-20-0
Molecular Formula:C₄₁H₄₂O₈S
Molecular Weight:694.846
Hs Code.:

Synonyms:2,6-anhydro-3,4,7-tri-O-benzyl-5-O-((2-naphthyl)methyl)-1-deoxy-1-ethoxysulfonyl-D-gluco-hept-1-enitol

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Chemical Property of 2,6-anhydro-3,4,7-tri-O-benzyl-5-O-((2-naphthyl)methyl)-1-deoxy-1-ethoxysulfonyl-D-gluco-hept-1-enitol

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Technology Process of 2,6-anhydro-3,4,7-tri-O-benzyl-5-O-((2-naphthyl)methyl)-1-deoxy-1-ethoxysulfonyl-D-gluco-hept-1-enitol

There total 7 articles about 2,6-anhydro-3,4,7-tri-O-benzyl-5-O-((2-naphthyl)methyl)-1-deoxy-1-ethoxysulfonyl-D-gluco-hept-1-enitol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 10.0%

: 774591-92-3
4-methoxyphenyl 2,3,6-tri-O-benzyl-β-D-glucopyranoside

: 1381871-18-6
ethyl 3,4,7-tri-O-benzyl-5-O-((2-naphthyl)methyl)-1-deoxy-1-ethoxysulfonyl-2-thio-α-D-gluco-hept-2-ulopyranoside

: 1381871-20-0
2,6-anhydro-3,4,7-tri-O-benzyl-5-O-((2-naphthyl)methyl)-1-deoxy-1-ethoxysulfonyl-D-gluco-hept-1-enitol

: 1381871-19-7
p-methoxyphenyl 3,4,7-tri-O-benzyl-5-O-((2-naphthyl)methyl)-1-deoxy-1-ethoxysulfonyl-α-D-gluco-hept-2-ulopyranosyl-(2->4)-2,3,6-tri-O-benzyl-β-D-glucopyranoside

Guidance literature:: With N-iodo-succinimide; trifluorormethanesulfonic acid; In dichloromethane; at -40 ℃; for 1.25h; Inert atmosphere;
DOI:10.1016/j.tet.2012.04.067

Reference yield:

: 774591-92-3
4-methoxyphenyl 2,3,6-tri-O-benzyl-β-D-glucopyranoside

: 1381871-17-5
3,4,7-tri-O-benzyl-5-O-((2-naphthyl)methyl)-1-deoxy-1-ethoxysulfonyl-α-D-gluco-hept-2-ulopyranosyl chloride

: 1381871-20-0
2,6-anhydro-3,4,7-tri-O-benzyl-5-O-((2-naphthyl)methyl)-1-deoxy-1-ethoxysulfonyl-D-gluco-hept-1-enitol

: 1381871-19-7
p-methoxyphenyl 3,4,7-tri-O-benzyl-5-O-((2-naphthyl)methyl)-1-deoxy-1-ethoxysulfonyl-α-D-gluco-hept-2-ulopyranosyl-(2->4)-2,3,6-tri-O-benzyl-β-D-glucopyranoside

Guidance literature:: With silver trifluoromethanesulfonate; In dichloromethane; toluene; at 0 ℃; for 120h; Inert atmosphere; Molecular sieve;
DOI:10.1016/j.tet.2012.04.067

Reference yield:

: 1381871-17-5
3,4,7-tri-O-benzyl-5-O-((2-naphthyl)methyl)-1-deoxy-1-ethoxysulfonyl-α-D-gluco-hept-2-ulopyranosyl chloride

: 1381871-21-1
p-methoxyphenyl 3,4,7-tri-O-benzyl-1-deoxy-1-ethoxysulfonyl-α-D-gluco-hept-2-ulopyranosyl-(2->4)-2,3,6-tri-O-benzyl-β-D-glucopyranoside

: 1381871-20-0
2,6-anhydro-3,4,7-tri-O-benzyl-5-O-((2-naphthyl)methyl)-1-deoxy-1-ethoxysulfonyl-D-gluco-hept-1-enitol

: 1381871-22-2
p-methoxyphenyl 3,4,7-tri-O-benzyl-5-O-((2-naphthyl)methyl)-1-deoxy-1-ethoxysulfonyl-α-D-gluco-hept-2-ulopyranosyl-(2->5)-3,4,7-tri-O-benzyl-1-deoxy-1-ethoxysulfonyl-α-D-gluco-hept-2-ulopyranosyl-(2->4)-2,3,6-tri-O-benzyl-β-D-glucopyranoside

Guidance literature:: With silver trifluoromethanesulfonate; In dichloromethane; toluene; at 0 ℃; for 120h; Inert atmosphere; Molecular sieve;
DOI:10.1016/j.tet.2012.04.067