17-azido-3,6,9,12,15-pentaoxaheptadecyl 2-acetamido-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranoside

Base Information

Chemical Name:17-azido-3,6,9,12,15-pentaoxaheptadecyl 2-acetamido-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranoside
CAS No.:178476-11-4
Molecular Formula:C₃₄H₅₀N₄O₁₁
Molecular Weight:690.791
Hs Code.:

Synonyms:17-azido-3,6,9,12,15-pentaoxaheptadecyl 2-acetamido-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranoside

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Chemical Property of 17-azido-3,6,9,12,15-pentaoxaheptadecyl 2-acetamido-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranoside

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Technology Process of 17-azido-3,6,9,12,15-pentaoxaheptadecyl 2-acetamido-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranoside

There total 12 articles about 17-azido-3,6,9,12,15-pentaoxaheptadecyl 2-acetamido-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 178476-04-5
17-bromo-3,6,9,12,15-pentaoxaheptadecyl 2-acetamido-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranoside

: 178476-11-4
17-azido-3,6,9,12,15-pentaoxaheptadecyl 2-acetamido-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranoside

Guidance literature:: With sodium azide; In N,N-dimethyl-formamide; at 70 ℃; for 1h;
DOI:10.1248/cpb.48.1256

Reference yield:

: 178476-03-4
17-bromo-3,6,9,12,15-pentaoxaheptadecyl 2-acetamido-3-O-benzyl-4,6-O-benzylidene-2-deoxy-β-D-glucopyranoside

: 178476-11-4
17-azido-3,6,9,12,15-pentaoxaheptadecyl 2-acetamido-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 87 percent / Et₃SiH; TfOH; molecular sieves 4 A / CH₂Cl₂ / 1 h / -78 °C

2: 98 percent / sodium azide / dimethylformamide / 1 h / 70 °C

With triethylsilane; sodium azide; trifluorormethanesulfonic acid; 4 A molecular sieve; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1248/cpb.48.1256

Reference yield:

: 100-39-0
benzyl bromide

: 178476-11-4
17-azido-3,6,9,12,15-pentaoxaheptadecyl 2-acetamido-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 85 percent / BaO, Ba(OH)2*8H₂O / dimethylformamide / Ambient temperature

2: 87 percent / Et₃SiH, TfOH, MS₄A / CH₂Cl₂ / -78 °C

3: 90 percent / LiN₃ / dimethylformamide

With triethylsilane; barium dihydroxide; lithium azide; trifluorormethanesulfonic acid; barium(II) oxide; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/S0960-894X(98)00488-0