syn-(E)-2-phenylmethylene-3-quinuclidone oxime hydrochloride

Base Information

Chemical Name:syn-(E)-2-phenylmethylene-3-quinuclidone oxime hydrochloride
CAS No.:78961-46-3
Molecular Formula:C₁₄H₁₆N₂O*ClH
Molecular Weight:264.755
Hs Code.:

Synonyms:syn-(E)-2-phenylmethylene-3-quinuclidone oxime hydrochloride

Suppliers and Price of syn-(E)-2-phenylmethylene-3-quinuclidone oxime hydrochloride

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Chemical Property of syn-(E)-2-phenylmethylene-3-quinuclidone oxime hydrochloride

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Technology Process of syn-(E)-2-phenylmethylene-3-quinuclidone oxime hydrochloride

There total 3 articles about syn-(E)-2-phenylmethylene-3-quinuclidone oxime hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 37.0%

: 24123-89-5
(Z)-2-benzylidene-1-azabicyclo[2.2.2]octan-3-one

: 78961-46-3
syn-(E)-2-phenylmethylene-3-quinuclidone oxime hydrochloride

: 78130-07-1
anti-(Z)-2-phenylmethylene-3-quinuclidone oxime

: 78121-28-5
syn-(Z)-2-phenylmethylene-3-quinuclidone oxime

Guidance literature:: With hydroxylamine hydrochloride; In methanol; for 4h; Heating;
DOI:10.1007/BF02464105

Reference yield:

: 1193-65-3
3-quinuclidinone hydrochloride

: 78961-46-3
syn-(E)-2-phenylmethylene-3-quinuclidone oxime hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: NaOH / aq. ethanol / Heating

2: 37 percent / hydroxylamine hydrochloride / methanol / 4 h / Heating

With sodium hydroxide; hydroxylamine hydrochloride; In methanol; ethanol; 1: Condensation / 2: Condensation;
DOI:10.1007/BF02464105

Reference yield:

: 100-52-7
benzaldehyde

: 78961-46-3
syn-(E)-2-phenylmethylene-3-quinuclidone oxime hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: NaOH / aq. ethanol / Heating

2: 37 percent / hydroxylamine hydrochloride / methanol / 4 h / Heating

With sodium hydroxide; hydroxylamine hydrochloride; In methanol; ethanol; 1: Condensation / 2: Condensation;
DOI:10.1007/BF02464105