5,6-DIHYDRO-4H-PYRROLO[3,2,1-IJ]QUINOLINE-2-CARBOXYLIC ACID

Base Information

• Chemical Name: 5,6-DIHYDRO-4H-PYRROLO[3,2,1-IJ]QUINOLINE-2-CARBOXYLIC ACID
• CAS No.: 117273-45-7
• Molecular Formula: C₁₂H₁₁NO₂
• Molecular Weight: 201.225
• Mol file: 117273-45-7.mol

Synonyms:5,6-dihydro-4H-pyrrolo[3,2,1-ij]quinoline-2-carboxylic acid

Chemical Property of 5,6-DIHYDRO-4H-PYRROLO[3,2,1-IJ]QUINOLINE-2-CARBOXYLIC ACID

Chemical Property:

• Vapor Pressure: 0mmHg at 25°C

Purity/Quality:

5,6-DIHYDRO-4H-PYRROLO-[3,2,1-IJ]-QUINOLINE-2-CARBOXYLIC ACID 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 5,6-DIHYDRO-4H-PYRROLO[3,2,1-IJ]QUINOLINE-2-CARBOXYLIC ACID

There total 3 articles about 5,6-DIHYDRO-4H-PYRROLO[3,2,1-IJ]QUINOLINE-2-CARBOXYLIC ACID which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-(3,4-dihydro-2H-[1]quinolylimino)-propionic acid → 5,6-dihydro-4H-pyrrolo[3,2,1-ij]quinoline-2-carboxylic acid (117273-45-7)

Guidance literature:

With hydrogenchloride;

DOI:10.1021/ja01277a033

Reference yield:

ethyl 5,6-dihydro-4H-pyrrolo[3,2,1-ij]-quinoline-2-carboxylate (97631-21-5) → 5,6-dihydro-4H-pyrrolo[3,2,1-ij]quinoline-2-carboxylic acid (117273-45-7)

Guidance literature:

ethyl 5,6-dihydro-4H-pyrrolo[3,2,1-ij]-quinoline-2-carboxylate; With potassium hydroxide; In tetrahydrofuran; methanol; at 50 ℃; for 2h;

With hydrogenchloride; In water; pH=1;

DOI:10.1021/jm501984f

Reference yield:

hydrogenchloride (7647-01-0,15364-23-5) + 2-(3,4-dihydro-2H-[1]quinolylimino)-propionic acid → 5,6-dihydro-4H-pyrrolo[3,2,1-ij]quinoline-2-carboxylic acid (117273-45-7)

Guidance literature:

DOI:10.1021/ja01277a033

upstream raw materials:

hydrogenchloride

ethyl 5,6-dihydro-4H-pyrrolo[3,2,1-ij]-quinoline-2-carboxylate

Downstream raw materials:

5,6-dihydro-4H-pyrrolo-[3,2,1-ij]quinoline

5,6-Dihydro-4H-pyrrolo[3,2,1-ij]quinoline-2-carboxylic acid (3,3-diphenyl-allyl)-amide

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