N-methylmorpholinium 3-cyano-4-(2-furyl)-6-oxo-1,4,5,6-tetrahydropyridine-2-thiolate

Base Information

• Chemical Name: N-methylmorpholinium 3-cyano-4-(2-furyl)-6-oxo-1,4,5,6-tetrahydropyridine-2-thiolate
• CAS No.: 1391631-81-4
• Molecular Formula: C₅H₁₁NO*C₁₀H₈N₂O₂S
• Molecular Weight: 321.4

Synonyms:N-methylmorpholinium 3-cyano-4-(2-furyl)-6-oxo-1,4,5,6-tetrahydropyridine-2-thiolate

Chemical Property of N-methylmorpholinium 3-cyano-4-(2-furyl)-6-oxo-1,4,5,6-tetrahydropyridine-2-thiolate

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Technology Process of N-methylmorpholinium 3-cyano-4-(2-furyl)-6-oxo-1,4,5,6-tetrahydropyridine-2-thiolate

There total 1 articles about N-methylmorpholinium 3-cyano-4-(2-furyl)-6-oxo-1,4,5,6-tetrahydropyridine-2-thiolate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-methyl-morpholine (109-02-4) + furfural (98-01-1) + cycl-isopropylidene malonate (2033-24-1) + Cyanothioacetamide (7357-70-2) → N-methylmorpholinium 3-cyano-4-(2-furyl)-6-oxo-1,4,5,6-tetrahydropyridine-2-thiolate (1391631-81-4)

Guidance literature:

In ethanol; Reflux;

DOI:10.1080/10426507.2016.1224877

Reference yield: 73.0%

N-methylmorpholinium 3-cyano-4-(2-furyl)-6-oxo-1,4,5,6-tetrahydropyridine-2-thiolate (1391631-81-4) + α-chloro-N-(2-ethylphenyl)acetamide (57503-02-3) → 2-{[3-cyano-4-(furan-2-yl)-6-oxo-1,4,5,6-tetrahydropyridin-2-yl]thio}-N-(2-ethylphenyl) acetamide

Guidance literature:

In ethanol; water; for 48h;

DOI:10.1134/S1070363221090073

Reference yield: 69.0%

N-methylmorpholinium 3-cyano-4-(2-furyl)-6-oxo-1,4,5,6-tetrahydropyridine-2-thiolate (1391631-81-4) + 2-chloro-N-(2-methylphenyl)acetamide (37394-93-7) → 2-{[3-cyano-4-(furan-2-yl)-6-oxo-1,4,5,6-tetrahydropyridin-2-yl]thio}-N-(2-methylphenyl)acetamide

Guidance literature:

In ethanol; water; for 48h;

DOI:10.1134/S1070363221090073

upstream raw materials:

4-methyl-morpholine

furfural

cycl-isopropylidene malonate

Cyanothioacetamide

Downstream raw materials:

ethyl 6-{[3-cyano-4-(2-furyl)-6-oxo-1,4,5,6-tetrahydropyridin-2-ylthio]methyl}-4-(4-methoxyphenyl)-1-methyl-2-oxo-1,2,3,4-tetrahydropyrimidine-5-carboxylate

7-(2-furyl)-2,2-dimethyl-3-[(4-methylphenyl)amino]-5-oxo-2,3,6,7-tetrahydro-5H-thiazolo[3,2-a]pyridine-8-carbonitrile

N-{4-[(8-cyano-7-(2-furyl)-2,2-dimethyl-5-oxo-2,3,6,7-tetrahydro-5H-thiazolo[3,2-a]pyridin-3-yl)amino]phenyl}acetamide

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