ethyl allyl-(1-phenylallyl)carbamate

Base Information

• Chemical Name: ethyl allyl-(1-phenylallyl)carbamate
• CAS No.: 1044148-50-6
• Molecular Formula: C₁₅H₁₉NO₂
• Molecular Weight: 245.321
• Mol file: 1044148-50-6.mol

Synonyms:ethyl allyl-(1-phenylallyl)carbamate

Chemical Property of ethyl allyl-(1-phenylallyl)carbamate

Chemical Property:

Purity/Quality:

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Technology Process of ethyl allyl-(1-phenylallyl)carbamate

There total 1 articles about ethyl allyl-(1-phenylallyl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

chloroformic acid ethyl ester (541-41-3) + (R)-N-allyl-1-phenylprop-2-en-1-amine (488151-84-4) → ethyl allyl-(1-phenylallyl)carbamate (1044148-50-6)

Guidance literature:

With triethylamine; In tetrahydrofuran; at 0 - 20 ℃; Inert atmosphere;

DOI:10.1021/ol801071y

Reference yield: 92.0%

ethyl allyl-(1-phenylallyl)carbamate (1044148-50-6) → ethyl 2-phenyl-2H-pyrrole-1(5H)-carboxylate (1044148-62-0)

Guidance literature:

With Grubbs catalyst first generation; In dichloromethane; for 24h; Reflux; Inert atmosphere;

DOI:10.1021/ol801071y

upstream raw materials:

chloroformic acid ethyl ester

(R)-N-allyl-1-phenylprop-2-en-1-amine

Downstream raw materials:

ethyl 2-phenyl-2H-pyrrole-1(5H)-carboxylate