diphenacyltellurium dibromide

Base Information

Chemical Name:diphenacyltellurium dibromide
CAS No.:120413-84-5
Molecular Formula:C₁₆H₁₄Br₂O₂Te
Molecular Weight:525.694
Hs Code.:

Synonyms:diphenacyltellurium dibromide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of diphenacyltellurium dibromide

Chemical Property:

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Technology Process of diphenacyltellurium dibromide

There total 5 articles about diphenacyltellurium dibromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 99766-21-9
diphenacyl telluride

: 120413-84-5
diphenacyltellurium dibromide

Guidance literature:: With bromine; In tetrachloromethane; Petroleum ether; at 20 ℃; for 2h;
DOI:10.1016/j.jorganchem.2003.10.021

Reference yield: 65.0%

: 70-11-1
α-bromoacetophenone

: 120413-84-5
diphenacyltellurium dibromide

Guidance literature:: With tellurium; Heating;

Reference yield:

: 70-11-1
α-bromoacetophenone

: 120413-84-5
diphenacyltellurium dibromide

Guidance literature:: Multi-step reaction with 4 steps

1.1: tellurium powder / dimethylsulfoxide / 1 h / Heating

1.2: 35 percent / dimethylsulfoxide / 2 h / 20 °C

2.1: NaOH in EtOH; O₂ / 0.83 h / 40 °C

2.2: 39 percent / NaOH in EtOH / 1 h / Heating

3.1: 67 percent / activated copper / dioxane / 3 h / Heating

4.1: 80 percent / Br₂ / diethyl ether

With sodium hydroxide; tellurium; bromine; oxygen; copper; In 1,4-dioxane; diethyl ether; dimethyl sulfoxide;
DOI:10.1016/S0022-328X(03)00152-9