octyl 2-O-benzoyl-4,6-O-(1,1,3,3-tetraisopropyl-1,3-disiloxanediyl)-1-thio-α-D-mannopyransoside

Base Information

Chemical Name:octyl 2-O-benzoyl-4,6-O-(1,1,3,3-tetraisopropyl-1,3-disiloxanediyl)-1-thio-α-D-mannopyransoside
CAS No.:187139-98-6
Molecular Formula:C₃₃H₅₈O₇SSi₂
Molecular Weight:655.056
Hs Code.:

Synonyms:octyl 2-O-benzoyl-4,6-O-(1,1,3,3-tetraisopropyl-1,3-disiloxanediyl)-1-thio-α-D-mannopyransoside

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Chemical Property of octyl 2-O-benzoyl-4,6-O-(1,1,3,3-tetraisopropyl-1,3-disiloxanediyl)-1-thio-α-D-mannopyransoside

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Technology Process of octyl 2-O-benzoyl-4,6-O-(1,1,3,3-tetraisopropyl-1,3-disiloxanediyl)-1-thio-α-D-mannopyransoside

There total 6 articles about octyl 2-O-benzoyl-4,6-O-(1,1,3,3-tetraisopropyl-1,3-disiloxanediyl)-1-thio-α-D-mannopyransoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 98-88-4
benzoyl chloride

: 187139-96-4
octyl 4,6-O-(1,1,3,3-tetraisopropyl-1,3-disiloxane-1,3-diyl)-1-thio-α-D-mannopyranoside

: 187139-98-6
octyl 2-O-benzoyl-4,6-O-(1,1,3,3-tetraisopropyl-1,3-disiloxanediyl)-1-thio-α-D-mannopyransoside

Guidance literature:: In pyridine; for 24h; Ambient temperature;
DOI:10.1016/S0008-6215(96)00215-7

Reference yield:

: 83-87-4,604-68-2,604-69-3,2152-77-4,4026-35-1,4163-59-1,4163-60-4,4163-61-5,4163-65-9,4257-94-7,4257-96-9,16299-15-3,19186-39-1,19189-55-0,25878-60-8,25941-03-1,32445-48-0,32445-49-1,32445-53-7,32445-54-8,34685-58-0,34685-59-1,43168-42-9,43168-44-1,43169-22-8,43169-25-1,66966-07-2,70749-17-6,80184-01-6,93221-01-3,93221-02-4,99630-88-3,109215-53-4,115792-70-6,115792-73-9,139894-92-1,139973-25-4,144071-49-8,147648-81-5
D-Mannose pentaacetate

: 187139-98-6
octyl 2-O-benzoyl-4,6-O-(1,1,3,3-tetraisopropyl-1,3-disiloxanediyl)-1-thio-α-D-mannopyransoside

Guidance literature:: Multi-step reaction with 4 steps

1: 52 percent / BF₃*Et₂O / CH₂Cl₂ / 24 h / Ambient temperature

2: 99 percent / NaOMe / methanol / 16 h / Ambient temperature

3: 5.51 g / imidazole / CH₂Cl₂; dimethylformamide / 0.25 h

4: 86 percent / pyridine / 24 h / Ambient temperature

With 1H-imidazole; boron trifluoride diethyl etherate; sodium methylate; In pyridine; methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/S0008-6215(96)00215-7

Reference yield:

: 111-88-6
Octanethiol

: 187139-98-6
octyl 2-O-benzoyl-4,6-O-(1,1,3,3-tetraisopropyl-1,3-disiloxanediyl)-1-thio-α-D-mannopyransoside

Guidance literature:: Multi-step reaction with 4 steps

1: 52 percent / BF₃*Et₂O / CH₂Cl₂ / 24 h / Ambient temperature

2: 99 percent / NaOMe / methanol / 16 h / Ambient temperature

3: 5.51 g / imidazole / CH₂Cl₂; dimethylformamide / 0.25 h

4: 86 percent / pyridine / 24 h / Ambient temperature

With 1H-imidazole; boron trifluoride diethyl etherate; sodium methylate; In pyridine; methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/S0008-6215(96)00215-7