(1S,2S)-N,N'-bis(bis(3,5-di-tert-butylphenyl)methyl)-1,2-diphenylethane-1,2-diamine

Base Information

Chemical Name:(1S,2S)-N,N'-bis(bis(3,5-di-tert-butylphenyl)methyl)-1,2-diphenylethane-1,2-diamine
CAS No.:1374447-29-6
Molecular Formula:C₇₂H₁₀₀N₂
Molecular Weight:993.599
Hs Code.:

Synonyms:(1S,2S)-N,N'-bis(bis(3,5-di-tert-butylphenyl)methyl)-1,2-diphenylethane-1,2-diamine

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Chemical Property of (1S,2S)-N,N'-bis(bis(3,5-di-tert-butylphenyl)methyl)-1,2-diphenylethane-1,2-diamine

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Technology Process of (1S,2S)-N,N'-bis(bis(3,5-di-tert-butylphenyl)methyl)-1,2-diphenylethane-1,2-diamine

There total 3 articles about (1S,2S)-N,N'-bis(bis(3,5-di-tert-butylphenyl)methyl)-1,2-diphenylethane-1,2-diamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: 62907-85-1
5,5'-(bromomethylene)bis(1,3-ditert-butylbenzene)

: 29841-69-8
(S,S)-1,2-diphenyl-1,2-diaminoethane

: 1374447-29-6
(1S,2S)-N,N'-bis(bis(3,5-di-tert-butylphenyl)methyl)-1,2-diphenylethane-1,2-diamine

Guidance literature:: With sodium carbonate; In 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone; at 120 ℃; for 2h; Inert atmosphere;
DOI:10.1016/j.tet.2012.03.107

Reference yield:

: 62907-83-9
bis(3,5-di(tert-butyl)phenyl)methanol

: 1374447-29-6
(1S,2S)-N,N'-bis(bis(3,5-di-tert-butylphenyl)methyl)-1,2-diphenylethane-1,2-diamine

Guidance literature:: Multi-step reaction with 2 steps

1: Acetyl bromide / benzene / 3 h / 0 °C / Inert atmosphere

2: sodium carbonate / 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone / 2 h / 120 °C / Inert atmosphere

With Acetyl bromide; sodium carbonate; In 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone; benzene;
DOI:10.1016/j.tet.2012.03.107

Reference yield:

: 1-bromo-3,5-di-tert-butylphenyl magnesium bromide

: 1374447-29-6
(1S,2S)-N,N'-bis(bis(3,5-di-tert-butylphenyl)methyl)-1,2-diphenylethane-1,2-diamine

Guidance literature:: Multi-step reaction with 3 steps

1.1: tetrahydrofuran / 1 h / 0 °C / Inert atmosphere

1.2: Inert atmosphere

2.1: Acetyl bromide / benzene / 3 h / 0 °C / Inert atmosphere

3.1: sodium carbonate / 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone / 2 h / 120 °C / Inert atmosphere

With Acetyl bromide; sodium carbonate; In tetrahydrofuran; 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone; benzene;
DOI:10.1016/j.tet.2012.03.107