N₁-{6-[(mesitylsulfonyl)amino]hexyl}-N₁-(2-methoxybenzyl)-2,4,6-trimethyl-1-benzenesulfonamide

Base Information

• Chemical Name: N₁-{6-[(mesitylsulfonyl)amino]hexyl}-N₁-(2-methoxybenzyl)-2,4,6-trimethyl-1-benzenesulfonamide
• CAS No.: 253877-86-0
• Molecular Formula: C₃₂H₄₄N₂O₅S₂
• Molecular Weight: 600.844

Synonyms:N₁-{6-[(mesitylsulfonyl)amino]hexyl}-N₁-(2-methoxybenzyl)-2,4,6-trimethyl-1-benzenesulfonamide

Chemical Property of N₁-{6-[(mesitylsulfonyl)amino]hexyl}-N₁-(2-methoxybenzyl)-2,4,6-trimethyl-1-benzenesulfonamide

Chemical Property:

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Technology Process of N₁-{6-[(mesitylsulfonyl)amino]hexyl}-N₁-(2-methoxybenzyl)-2,4,6-trimethyl-1-benzenesulfonamide

There total 1 articles about N₁-{6-[(mesitylsulfonyl)amino]hexyl}-N₁-(2-methoxybenzyl)-2,4,6-trimethyl-1-benzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

2-mesitylenesulphonyl chloride (773-64-8) + N1-(2-methoxy-benzyl)-hexane-1,6-diamine; compound with GENERIC INORGANIC NEUTRAL COMPONENT → N1-{6-[(mesitylsulfonyl)amino]hexyl}-N1-(2-methoxybenzyl)-2,4,6-trimethyl-1-benzenesulfonamide (253877-86-0)

Guidance literature:

With sodium hydroxide; In dichloromethane; at 0 - 20 ℃; for 24h;

DOI:10.1021/jm991110n

Reference yield: 70.0%

bis(4-bromomethylphenyl)methane (16980-01-1) + N1-{6-[(mesitylsulfonyl)amino]hexyl}-N1-(2-methoxybenzyl)-2,4,6-trimethyl-1-benzenesulfonamide (253877-86-0) → N1-{6-[(mesitylsulfonyl)(4-{4-[((mesitylsulfonyl){6-[(mesitylsulfonyl)(2-methoxybenzyl)amino]hexyl}amino)methyl]benzyl}benzyl)amino]hexyl}-N1-(2-methoxybenzyl)-2,4,6-trimethyl-1-benzenesulfonamide (253877-87-1)

Guidance literature:

N₁-{6-[(mesitylsulfonyl)amino]hexyl}-N₁-(2-methoxybenzyl)-2,4,6-trimethyl-1-benzenesulfonamide; With sodium hydride; In N,N-dimethyl-formamide; at 20 ℃; for 1h;

bis(4-bromomethylphenyl)methane; In N,N-dimethyl-formamide; at 85 ℃; for 20h;

DOI:10.1021/jm991110n

Reference yield:

N1-{6-[(mesitylsulfonyl)amino]hexyl}-N1-(2-methoxybenzyl)-2,4,6-trimethyl-1-benzenesulfonamide (253877-86-0) → N1-(2-methoxybenzyl)-N6-(4-{4-[({6-[(2-methoxybenzyl)amino]hexyl}amino)methyl]benzyl}benzyl)-1,6-hexanediamine

Guidance literature:

Multi-step reaction with 2 steps

1.1: NaH / dimethylformamide / 1 h / 20 °C

1.2: 70 percent / dimethylformamide / 20 h / 85 °C

2.1: HBr; PhOH; AcOH / 0 - 20 °C

With hydrogen bromide; sodium hydride; acetic acid; phenol; In N,N-dimethyl-formamide; 1.1: Metallation / 1.2: Alkylation / 2.1: Hydrolysis;

DOI:10.1021/jm991110n

upstream raw materials:

2-mesitylenesulphonyl chloride

Downstream raw materials:

N₁-{6-[(mesitylsulfonyl)(4-{4-[((mesitylsulfonyl){6-[(mesitylsulfonyl)(2-methoxybenzyl)amino]hexyl}amino)methyl]benzyl}benzyl)amino]hexyl}-N₁-(2-methoxybenzyl)-2,4,6-trimethyl-1-benzenesulfonamide

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